The releases of harmful ions from cobalt based alloy to host tissues have raised significant health concerns. Carbon contents in this alloy may influence ions release but has yet investigated. It is hypothesized that carbon contents in this alloy will help the formation of oxide layer during thermal oxidation process and hence reducing the release of Co/Cr ions after implantation. In this study, Co-Cr-Mo alloy with carbon concentrations of 0.03% and 0.24% were oxidized at 1050°C for 3 hours under atmospheric condition. The oxidized substrates were characterized under FESEM and subjected to circulating immersion test in simulated body fluid (SBF) for 21 days. Metal ions release was measured using inductively coupled plasma-mass spectrometry (ICP-MS) at day 0, 7, 14 and 21. Oxidized high carbon samples show denser and a more uniform oxide layer than samples with low carbon contents. It is found that compact oxide structure promotes less metal ions release during immersion.
Cathodic arc physical vapor deposition (CAPVD) is one of the physical Vapor deposition (PVD) techniques used to coat titanium nitride (TiN) on biomedical implants due to its good adhesion and high evaporation rate. However, this technique emits micro droplets which have can detrimental effect on the coating performance. Previous studies reported that micro droplets can be controlled through proper deposition parameters. In this paper, the PVD coating was performed on the Ti-13Zr-13Nb biomedical alloy with different substrate temperatures. Scanning electron microscopy (SEM) was used to characterized the surface morphology and coating thickness while X-Ray Diffraction (XRD was employed to evaluate the crystal phase of the coated substrates. Image analysis software was used to quantify micro droplets counts. The results show that higher substrate temperature able to decrease a significant amount of micro droplets and concurrently increase the thickness of TiN coating. A mixed crystal planes of (111) and (200) are obtained on the coated substrates at this setting which exhibits denser structure as compared to substrates coated at lower substrate temperature.
Recently, Composite Sandwich Panel (CSP) technology considerably influenced the design and fabrication of high performance structures. Although using CSP increases the reliability of structure, the important concern is to understand the complex deformation and damage evolution process. This study is focused on the flexural and indentation behavior of CSP made of chopped strand mat glass fiber and polyester matrix as face sheets and polyurethane foam as foam core subject to flexural and indentation loading condition. A setup of three-point bending and indentation test is prepared using different strain rates of 1mm/min, 10mm/min, 100mm/min and 500mm/min to determine the effects of strain rate on flexural and indentation behavior of CSP material. The load-extension, stress-extension response and energy absorption of the panel show the relation between the flexural and indentation behavior of panels to strain rate as by increasing the strain rate, the flexural properties and the energy absorption of panel are increased.
Lost foam casting is a relatively new process in commercial terms and is widely used to produce defect free castings owing to its advantages like producing complex shape and acceptable surface finish. In the present research, experimental investigations in lost foam casting of aluminium-silicon cast alloy, LM6, were conducted. The main objective of the study was to evaluate the effect of different sand sizes and pouring temperatures on the porosity of thin-wall castings. A stepped pattern was used in the study and the focus of the investigations was at the thinnest 3 mm section. A full 2-level factorial design experimental technique was employed to plan the experiment and subsequently identify the significant factors which affect the casting porosity. The result shows that increasing in the pouring temperature decreases the porosity in the thin-wall section of casting. Finer sand size is more favourable than coarse size for LFC mould making process.
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