Abstract. Caesium lutetium hexaniobium octadecachloride, M r = 1503.46, hexagonal, P31c, a = 9.1882 (7), c= 17.1681 (3)A, V= 1255.2 (2)A 3, z=2, D x = 3.978 g cm -3, 2(Mo Ka) = 0-71073 A, # = 97.866 cm -~, F(000) = 1356, R = 0.022 (wR = 0.027) for 1131 independent reflections. The structure is built up from ([Nb6C1~21C16) 4-units, linked together by Lu atoms lying in a slightly distorted chlorine octahedron. The Cs atoms are surrounded by twelve CI atoms also belonging to six adjacent (Nb6CI~8) units.
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