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Fatigue failure processes in metallic materials are closely related to the evolution of strain localisation under cyclic loading. Characterisation of this strain localisation is important in understanding the mechanisms of fatigue crack initiation and propagation, and provides critical validation data to develop appropriate crystal plasticity models for prediction of these processes. In this study, strain localisation during fatigue crack initiation and early crack propagation in an advanced Ni-based superalloy for turbine disc application has been characterised at the grain level with a sub-micron resolution by digital image correlation on SEM images using secondary γ' themselves as the speckle pattern. The obtained full-field strains have been analysed in global coordinates associated with the applied loading direction and in terms of the local coordinates associated with individual slip bands. Deformation arising from in-plane and out-of-plane dislocation slip can be identified by a combination of shear strain ɛ xy and transverse strain ɛ yy in the local slip band coordinates in combination with EBSD analysis. Cracks preferentially initiate from slip/strain bands adjacent and parallel to twin boundaries and then propagate along the slip/strain bands, leading to the onset of significant transverse strain ɛ yy in the local band coordinates as a consequence of crack opening. Crack propagation is closely related to strain accumulation at the crack tip which is determined by the grain orientation and grain size. Transverse strain ɛ yy in local slip band coordinates together with the inclination angle between dislocation slip direction on an activated {111} plane and the slip trace of this {111} plane at the specimen surface is proposed to be a cracking indicator/fracture criterion.

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Abstract:Fatigue crack initiation and propagation behaviour in subsolvus heat treated turbine disc alloy N18 has been assessed in air and vacuum at 650 and 725 o C under three-point loading.Fatigue crack initiation processes have been evaluated using single edge U-notch specimens under a 1-1-1-1 trapezoidal loading waveform along with interrupted tests at 650 o C to allow intermittent observations of the notch surface. The results show apparent grain boundary (GB) oxidation can occur under an oxygen partial pressure of 10 -2~1 0 -3 Pa. Cracks mainly initiate from grain boundaries or γ/γʹ interfaces due to the formation and subsequent cracking of Crrich and/or Co-rich oxides, and occasionally initiate from surface pores. Fatigue life in these tests appears to be dominated by this crack initiation process and is significantly reduced by increasing temperature and/or application of an oxidizing environment. Crack growth tests conducted under 1-1-1-1 and 1-20-1-1 loading waveforms indicate that oxidation significantly degrades the crack growth resistance of N18 and is associated with more intergranular fracture surface features. Additional oxidation effects on propagation caused by higher temperature or prolonging dwell time appear limited, whereas a prolonged dwell period seems to instead promote additional creep process, which further enhance crack growth, especially at higher temperature.

Ni-based superalloys in turbine disc applications face increasing susceptibility to oxygen-assisted fatigue crack propagation due to increased turbine entry temperatures. The continued lack of understanding of the interplay between the factors operating during oxygen-assisted fatigue crack propagation limits: (1) development of lifing methodologies to accurately predict the fatigue performance of disc alloys/components and (2) associated disc alloy developments. An underpinning requirement to better understand the role of oxygen is to characterise the process of oxygen diffusion in the localised stress/strain state at the crack tip, which is related closely to microstructural features. The link between three-dimensional crack tomography, crack propagation rate and oxygen-related attack needs to be established. Quantitative models which include the interaction between fatigue-creep-oxygen attack need further development.