On a site in the Sudan Savanna, chemical properties of soils (except for phosphate) and the composition of cotton leaves were determined after fifteen annual treatments including dung, ammonium sulphate, single superphosphate and potassium chloride, in all combinations of three levels. In the soils dung increased C, N, cation exchange capacity, exchangeable Ca and Mg and pH, and decreased soluble Al and Mn; ammonium sulphate decreased pH, increased soluble Al and Mn, and decreased exchangeable Ca and Mg; potassium chloride had no obvious effects. In the plants dung increased P and reduced Mn; ammonium sulphate reduced Ca and Mg, and increased Mn; superphosphate increased P, Ca and Mg, and reduced K; potassium chloride increased K slightly. The most important results were the ability of ammonium sulphate to acidify the soil, as shown by soil properties and reflected in tissue composition, and the ability of dung to ameliorate these effects. Reduction of crop yield in the presence of adequate nutrient supply seems to have been due to excessive soil acidity.In 1949-50 a number of manurial trials, designed to test the effects of four materials separately and in all combinations, were started in Northern Nigeria. The materials and their rates of application were: D-Dung (cattle pen manure) o, 1 and 2 tons/acre N-Ammonium sulphate (21 %N) o, 50 and 100 lb/acre P-Single superphosphate (8-7%P) o, 50 and 100 lb/acre K-Potassium chloride (42%K) 0, 25 and 50 lb/acre.A 3 4 factorial design was used and the total of 81 plots was arranged in 9 blocks. Plot size was 1/20 acre, with adequate discards, and each plot received the same manurial treatment each year. Many of these trials were stopped in 1957, and Obi (1959) summarized the effects on crop yields up to that time, but three of them were continued. The trial at Samaru has been mono-cropped with sprayed cotton since 1961, and this paper reports the effects of the fertilizer and manure treatments on some chemical properties of the soil and on the composition of leaf samples from the cotton crop with respect to certain chemical elements.
MATERIALS AND METHODSThe site of the experiment is within the Sudan Savanna zone and has a light brown loamy fine sand topsoil, with a sharp boundary at about 8-9 in. to a loam/sandy clay loam subsoil. Acid metamorphic rocks are thought to underlie the site, but the soil also incorporates a considerable amount of drift material.