Inline holography, like other lensless imaging methods, circumvents limitations of x-ray optics through an a posteriori phase-retrieval step. However, phase retrieval for optically thick, i.e., strongly absorbing and phase shifting, specimens remains challenging. In this paper, we demonstrate that near-field ptychography can be used to efficiently perform phase retrieval on a uranium sphere with a diameter of about 46 μm, which acts as an optically thick sample. This particular sample was not accessible by inline holography previously. The reconstruction is based on a statistical model and incorporates partial coherence by decomposing the illumination into coherent modes. Furthermore, we observe that phase vortices, which can occur as artifacts during the reconstruction, pose a greater challenge than in far-field methods. We expect that the methods described in this paper will allow production of reliable phase maps of samples which cannot be accessed by inline holography.
Although many of the instruments planned for the TMT (Thirty Meter Telescope) have their own closely-coupled adaptive optics systems, TMT will also have a facility Adaptive Optics (AO) system, NFIRAOS, feeding three instruments on the Nasmyth platform. This Narrow-Field Infrared Adaptive Optics System, employs conventional deformable mirrors with large diameters of about 300 mm. The requirements for NFIRAOS include 1.0-2.5 microns wavelength range, 30 arcsecond diameter science field of view (FOV), excellent sky coverage, and diffraction-limited atmospheric turbulence compensation (specified at 133 nm RMS including residual telescope and science instrument errors.) The reference design for NFIRAOS includes six sodium laser guide stars over a 70 arcsecond FOV, and multiple infrared tip/tilt sensors and a natural guide star focus sensor within instruments. Larger telescopes require greater deformable mirror (DM) stroke. Although initially NFIRAOS will correct a 10 arcsecond science field, it uses two deformable mirrors in series, partly to provide sufficient stroke for atmospheric correction over the 30 m telescope aperture, but mainly to improve sky coverage by sharpening near-IR natural guide stars over a 2 arcminute diameter "technical" field. The planned upgrade to full performance includes replacing the ground-conjugated DM with a higher actuator density, and using a deformable telescope secondary mirror as a "woofer." NFIRAOS feeds three live instruments: a near-Infrared integral field Imaging spectrograph, a near-infrared echelle spectrograph, and after upgrading NFIRAOS to full multi-conjugation, a wide field (30 arcsecond) infrared camera.
Propagation-based imaging or inline holography in combination with computed tomography (holotomography) is a versatile tool to access a sample's three-dimensional (3D) micro or nano structure. However, the phase retrieval step needed prior to tomographic reconstruction can be challenging especially for strongly absorbing and refracting samples. Near-field ptychography is a recently developed phase imaging method that has been proven to overcome this hurdle in projection data. In this work we extend near-field ptychography to three dimensions and we show that, in combination with tomography, it can access the nano structure of a solid oxide fuel cell (SOFC). The quality of the resulting tomographic data and the structural properties of the anode extracted from this volume were compared to previous results obtained with holotomography. This work highlights the potential of 3D near-field ptychography for reliable and detailed investigations of samples at the nanometer scale, with important applications in materials and life sciences among others.
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