Portable X‐ray fluorescence (pXRF) is now widely used for detecting the elemental composition of a material. Elemental analysis can enhance archaeological interpretations, such as mapping, preservation analysis and identifying anthropogenic activities. However, validated and reproducible protocols for analysing archaeological soil are still required. The elemental concentrations detected with three sets of preparation methods were compared: in‐situ (no preparation), in‐field (analysing through plastic bags) and ex‐situ analysis (laboratory‐based preparation). Influential factors were also investigated: calibration parameter, moisture, homogeneity, sieve size and soil type. In‐field analysis attempted to improve reliability without offsite processing, but instead substantially reduced elemental concentrations and skewed the proportional distributions. Ex‐situ analysis significantly increased elemental concentrations and reduced variation. Proportional distribution was different between the three methods, but unchanged following homogenizing and sieving. These comparisons demonstrated that ex‐situ analysis maximizes detection and ensures consistent samples.

Waterlogged burial conditions impact upon artefact preservation. One major determinant of preservation is presence and behaviour of microorganisms, however, unravelling the mechanisms, especially in waterlogged conditions is challenging. In this study, we analysed elemental composition, bacterial diversity and community structure from excavation trenches at the Roman Site of Vindolanda, Northumberland, UK, using pXRF and 16S rRNA gene amplicon sequencing. Excavation trenches provide information of different occupation periods. The results indicated that microbial communities were dominated by Firmicutes, Bacteroidetes and Proteobacteria at a phylum level. Samples which also had visible vivianite presence showed that there were marked increases in Methylophilus. Methylophilus might be associated with favourable preservation in these anaerobic conditions. More research is needed to clearly link the presence of Methylophilus with vivianite production. The study emphasises the need for further integration of chemical and microbiome approaches, especially in good preservation areas, to explore microbial and chemical degradation mechanisms.

Museums have an ethical code of research and education, and 3D imaging has great potential in helping to achieve some of these objectives by providing accurate replications without barriers to access. Digital and printed models may remove object authenticity, but they do provide direct encounters with heritage and archaeological science whilst preserving the archaeological record. To demonstrate the potential for 3D imaging in archaeology and public engagement, this paper investigated an Ox cranium used for target practice at Vindolanda, Northumberland, UK. Vindolanda is a World Heritage Site on the Frontiers of the Roman Empire, known for its exceptional preservation of artefacts. The trauma type, shaping, impact direction and mortem period were identified, followed by comparisons and physical fits with weaponry used by the military at Vindolanda. The digital and printed models provide effective tools for displaying this evidence within the context of Roman archery to the public. The cranium had evidence of repeated target practice from arrows and potentially lances. The fragmentation of the trauma was angled internally, showing that the arrows were aimed from the front and toward the facial area of the Ox. The high-precision of the archers had separated the lower right portion of the facial area from the rest of the cranium. Several arrowhead sites and two lance head sites overlapped with little additional destruction, showing that some weapons were removed and retargeted. These features provide supporting evidence of individuals in the Roman military at Vindolanda actively participating in high-level archery target practice. The success of this pilot study will be developed to produce 3D models of the crania recovered from Vindolanda for the public to directly interact with this complex, contextual information for deep and effective learning.

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