This paper presents the mechanical and tribological characteristics of potassium titanate whisker (PTW) reinforced epoxy composites. The effect of various test variables and material parameters on the friction and wear behavior of epoxy/PTW composites has been studied systematically. Tribological tests were conducted on a pin-on-disc apparatus under dry sliding conditions. Addition of PTW was found to improve the wear resistance of the composites and 15 wt% PTW filled epoxy exhibited lowest specific wear rate and highest friction coefficient compared to other test samples. PTW additions showed beneficiary effect on density, hardness, and stiffness properties of composites; however, strength properties and ductility were found to decrease with the increasing content of PTW. Scanning electron microscope (SEM) images of tensile fractured surfaces and worn-out surfaces of selected samples revealed different fracture mechanisms.
This study evaluates the influence of independent parameters such as sliding velocity (A), normal load (B), filler content (C), and sliding distance (D) on wear performance of potassium-titanate-whiskers (PTW) reinforced epoxy composites using a statistical approach. The PTW were reinforced in epoxy resin to prepare whisker reinforced composites of different compositions using vacuum-assisted casting technique. Dry sliding wear tests were conducted using a standard pin on disc test setup following a well planned experimental schedule based on Taguchi’s orthogonal arrays. With the signal-to-noise (S/N) ratio and analysis of variance (ANOVA) optimal combination of parameters to minimize the wear rate was determined. It was found that inclusion of PTW has greatly improved the wear resistance property of the composites. Normal load was found to be the most significant factor affecting the wear rate followed by (C), (D), and (A). Interaction effects of various control parameters were less significant on wear rate of composites.
The dry sliding friction and wear behavior of epoxy hybrid composites reinforced with glass fibers and a varying amount of potassium titanate whiskers (PTWs) fabricated by vacuum hand layup method were studied. The influence of normal load, sliding velocity, and whisker content on both friction coefficient and specific wear rate was investigated on a pin-on-disc machine. The tests were conducted at ambient conditions based on the 3 × 3 (3 factors at 3 levels) full factorial design. Analysis of variance (ANOVA) was performed to obtain the contribution of control parameters on friction coefficient and wear rate. The density and hardness of the composites were found to be enhanced with the PTW loading. The friction coefficient and wear resistance of the hybrid composites were found to be improved with the whisker content and were also greatly influenced by normal load and sliding velocity. A correlation between dry sliding wear behaviors of composites with wear parameters was obtained by multiple regressions. The worn out surface of selected samples was observed under scanning electron microscope (SEM) to identify wear mechanisms. This study revealed that the addition of the ceramic microfillers such as PTW improves the wear performance of the epoxy/glass polymer composites significantly.
Metal ceramic crowns obtained from direct optical scanning showed the least marginal and internal gap when compared to the castings obtained from inlay casting wax and indirect optical scanning. Indirect and direct optical scanning had yielded results within clinically acceptable range.
Purpose This paper aims to report the effect of titanium oxide (TiO2) particles on the physical, mechanical, tribological and water resistance properties of 5% NaOH-treated bamboo fiber–reinforced composites. Design/methodology/approach In this research, the epoxy/bamboo/TiO2 hybrid composite filled with 0–8 Wt.% TiO2 particles has been fabricated using simple hand layup techniques, and testing of the developed composite was done in accordance with the American Society for Testing and Materials (ASTM) standard. Findings The results of this study indicate that the addition of TiO2 particles improved the mechanical properties of the developed epoxy/bamboo composites. Tensile properties were found to be maximum for 6 Wt.%, and impact strength was found to be maximum for 8 Wt.% TiO2 particles-filled composite. The highest flexural properties were found at a lower TiO2 fraction of 2 Wt.%. Adding TiO2 filler helped to reduce the water absorption rate. The studies related to the wear and friction behavior of the composite under dry and abrasive wear conditions reveal that TiO2 filler was beneficial in improving the wear performance of the composite. Originality/value This research paper attempts to include both TiO2 filler and bamboo fibers to develop a novel composite material. TiO2 micro and nanoparticles are promising filler materials; it helps to enhance the mechanical and tribological properties of the epoxy composites and in literature, there is not much work reported, where TiO2 is used as a filler material with bamboo fiber–reinforced epoxy composites.
Untreated and alkaline treated bamboo and flax fiber reinforced epoxy composites are processed using a hand layup process. The effect of alkaline treatment on the mechanical properties of the composites has been analysed. Alkaline treatment of the fiber has enhanced the mechanical properties of the developed composites. Composite reinforced with 5 % NaOH treated fiber show better performance when compared with untreated fiber reinforced composites. Alkaline treatment of the bamboo and flax fiber with 5 % NaOH has improved the hardness by 3.57 and 2.43 %, tensile strength by 47 and 20.72 % and flexural strength by 7.36 and 13.85 % in bamboo and flax fiber reinforced composites, respectively. The increase in the percentage NaOH in the alkaline treatment of the fibers resulted in weakening of fiber resulting in a drop in the properties of the developed composites. Water absorption tests of the developed composites were conducted as per ASTM D570 by immersion in distilled water at room temperature. The influence of water absorption on mechanical properties of developed composites is also examined. The quantity of water absorption and diffusion coefficient are reduced with alkaline treatment of fiber. Mechanical properties of the composite were found to decrease by the water absorption, which can be controlled by alkaline treatment of fiber and thereby reducing water absorption rate and improve the mechanical properties of the composites. HIGHLIGHTS Reinforcing natural fiber in polymer resin is highly beneficial because it helps to improves the strength and toughness of the polymer Moisture absorption rate and lack of interfacial adhesion between the polymer and natural fiber made natural fiber reinforced composites less attractive compared to synthetic fiber reinforced composites Alkaline treatment of the natural fiber increases the fiber surface roughness, which results in improved mechanical interlock between fiber and matrix, resulting in improved mechanical and water resistance properties of the developed composites GRAPHICAL ABSTRACT
The scarcity of conventional fuel and stringent emission norms made researchers to look after alternative fuels to run an internal combustion engine. One of the possible alternatives for the Compression Ignition engine is biodiesel. Although there are some challenges such as high viscosity, low calorific value, carbon deposit on the injector nozzle, etc. To overcome these challenge nanoparticles are added which will bring most properties near to virgin diesel. Simarouba a non-edible biodiesel feedstock used and aluminum oxide nanoparticles are added with 50 nm size. Using a probe-type Ultrasonication process nano-biodiesel blend is prepared. To improve stability SDS surfactants are added. The characterization of nanoparticles studied using SEM image. The performance of the engine tested for different dosage levels of nanoparticles mainly 25 ppm, 50 ppm, and 75 ppm. The injection timing, injector pressure, and speed kept constant, whereas injection pressure is varied 200 bar, 225 bar, and 250 bar. There is found a 5.2% increase in brake thermal efficiency for nanoparticles added blend biodiesel at 250 bar compare to 200 bar pressure. For the same thing brake specific fuel consumption decreased by 9%. Most of emissions such as Carbon monoxide, unburnt hydrocarbons decreased, whereas there is a significant amount of increase in oxides of nitrogen emission found.
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