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The formation and reactivity of a stable oxygen species which is effective in the production of hydrocarbons from methane at lower than normal temperatures is described.

The sorption of the title compound into the pores of NaY zeolite is studied by i.r. and 13C magic angle spinning n.m.r. spectroscopy; after appropriate activation, the supported cobalt system is a shape-selective catalyst for the hydrogenation of carbon monoxide to alkenes with a cut-off at Cg.