The determination method for analyzing trace copper in vanadium alloy by flame atomic absorption spectrometry was investigated in the paper. The sample digestion method, digestion acidity, determination conditions, matrix interferences, method precision, recovery of standard addition were investigated in detail. The method precision in RSD% was 8.6%, and the average recoveries of standard addition were from 93.9% to 95.6%. The experimental results indicated that the proposed method for determination of trace copper in vanadium alloy was simple, fast, accurate, and easy to operate, which was suitable for quality control of vanadium alloy.
A multi-scale method was developed, which utilized intrinsic relationships among zeta potential of particles, rheological properties of suspensions and particle size distribution (PSD), to analyze dispersion behavior of nanoparticles in concentrated suspensions. It was found that PSD of a kind of nanoceria particles by dynamic light scattering (DLS) method in solution A with concentration 5 wt% accorded well with that by direct TEM analysis, which meant the particles had been dispersed well. However, there had a significant difference when the concentration was increased to 20 wt%. When particles concentration increased from 5 wt% to 20 wt%, zeta potential in solution A changed from-150 mV to-100 mV, while zeta potential in solution B changed from-35mV to-45 mV. Variations of zeta potential of particles accorded well with rheological properties of suspensions too, from phenomenological models. When the suspensions composed by solution A and the nanoparticles with concentration about 20 wt% was diluted with its original solution to 5 wt%, the PSD of nanoceria could be measured indirectly, which accorded well with both that of a suspension prepared directly with near concentration and that from TEM images. Then a method to measure PSD of nanoparticles in concentrated suspension was brought forward.
The wave-like Ni is synthesized without any impurity via varying the addition of surfactant PVP, its microwave absorption can be attributed to dielectric loss and magnetic loss, and exhibits an maximum absorption value of -14.19 dB at 14.2 GHz.
Nano-indentation technology was brought to study microscopic mechanical properties of a single-crystalline diamond (SCD). Nano-indentation measurement was conducted on the {100} plane of SCD, and influences of various factors on measured results were analyzed, from which methods were confirmed to improve veracity of measurement. Properties of the indenter were checked with a fused silica sample both before and after indentation on diamond, which provided guarantee to veracity of results on diamond. It was found that tilt of diamond surface had so great influence that it could damage the indenter, and make the indentation curves anomalous. While damage of indenter could be avoided and valid measurement results could be obtained when tilt of diamondsurface was decreased below 0.10º and the maximal indentation force was less than 10 mN. Deformation of the diamond was almost full-elastic during indentation process. Indentation hardness of {100} plane of the SCD was about 70 GPa with standard deviation less than 3 GPa. And there had good reproducibility between two groups of measurements.
Magnetorheological (MR) fluids can transform from fluid to solid and back to fluid rapidly in magnetic field. It is a novel intelligent phase transition material. In this study, MR fluids are filled inside a thin wall spherical shell as phase transition material to improve the workpiece stiffness. A fixture structure based on MR fluids for the thin wall spherical shell precision machining is designed. The fixture stiffness can be controlled and the MR fluids can be used many times. The MR fluid as strengthening material is developed and the amount of metal powder in MR fluids is 52% by volume and the performance of MR fluids is measured. Based on electromagnetic principle, a special magnetic field is designed and the magnetic field distributing is analyzed and optimized. The thin wall spherical shell using the designed fixture is turned in CK7820B lathe. The cutting experiment result shows that the fixture based on MR fluids can improve the workpiece machining precision.
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