Plenty of studies have been performed to probe the diverse properties of ZnO nanowires, but only a few have focused on the physical properties of a single nanowire since analyzing the growth mechanism along a single nanowire is difficult. In this study, a single ZnO nanowire was synthesized using a Ti-assisted chemical vapor deposition (CVD) method to avoid the appearance of catalytic contamination. Two-dimensional energy dispersive spectroscopy (EDS) mapping with a diffusion model was used to obtain the diffusion length and the activation energy ratio. The ratio value is close to 0.3, revealing that the growth of ZnO nanowires was attributed to the short-circuit diffusion.
In this work, we succeeded in preparing in-plane zinc oxide nanowires using a Ti-grid assisted by the chemical vapor deposition method. Optical spatial mapping of the Confocal Raman spectra was used to investigate the phonon and geometric properties of a single ZnO nanowire. The local optical results reveal a red shift in the non-polar E2 high frequency mode and width broadening along the growth direction, reflecting quantum-confinement in the radial direction.
We report on the formation and spontaneous self-organization of Cu(2)O/CuO core-shell nanowires from individual copper nanoparticles. The growth process is interpreted using the results of time-dependent in situ x-ray diffraction. High-resolution transmission electron microscopy is used to observe the intermediate state of pearl-necklace-like aggregates that form a chain-like configuration of Cu(2)O nanoparticles intertwined into nanowires. The existence of an amorphous CuO shell is confirmed by the XANES technique and explained through an intensity simulation using a proposed core-shell nanowire model.
We review the phenomenology of the exchange bias and its related effects in core–shell nanocrystals. The static and dynamic properties of the magnetization for ferromagnetic Ni-core and antiferromagnetic NiO-shell cluster glassy nanoparticles are examined, along with the pinning–depinning process, through the measurement of the conventional exchange bias, and associated with different cooling fields and particle sizes. Two significant indexes for the dipolar interaction n and multi-anisotropic barrier β derived from the dynamic magnetization are proposed, which provide a unified picture of the exchange bias mechanism and insight into the influence of the cooling field.Electronic supplementary materialThe online version of this article (doi:10.1186/s11671-015-0925-0) contains supplementary material, which is available to authorized users.
Single crystal InSn nanocubes were synthesized using a simple thermal evaporation method and observed using high-resolution transmission electron microscope images. Enhanced superconducting transitions were observed from the magnetization, revealing a main diamagnetic Meissner state below 6.02(5) K with β-InSn phase. The transition temperature reduced to zero as the applied magnetic field Ha neared 2 T and a critical field HC0 = 2.05(5) T was obtained. An extremely weak superconducting strength α = 0.35 was obtained and revealed the coupling strength in InSn nanocubes to be weakened more than the BCS expectations indicated.
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