The aim of this work is to characterize the moisture-dependent actuation behavior of bioinspired and additively manufactured hygromorphs based by following deductive and inductive design approaches. Fused Filament Fabrication (FFF) is employed to print bilayered structures consisting of swellable active layers and rigid passive layers. The active layer is composed of a polylactic acid (PLA) matrix filled with different hygroscopic cellulosic materials (native and modified) up to a filler content of 50 m%. Acrylonitrile Butadiene Styrene (ABS) is used for the passive layer. The FFF process allows the generation of desired differential swelling properties in the composites upon moisture absorption. The moisture dependent actuation strain of the printed bilayers was determined by video analyses. Some influencing geometrical factors which contribute to the actuation were deduced from x-ray diffraction (XRD) and micro computed tomography (μCT). The investigation of the mean cellulose microfibril orientation on the surface of the active layer suggested a preferential orientation with respect to printing direction. Furthermore, a gradient of cellulosic material within a single printed layer was observed, which indicates fiber sedimentation. Comparison with the thermomechanical model derived from Timoshenko (1925) shows that the computational prediction of the moisture dependent actuation is considerably accurate for most selected cellulosic materials and filler contents.
After an incremental development which took place over four decades, X-ray imaging has become an important tool for non-destructive testing and evaluation. Computed Tomography (CT) in particular beholds the power of determining the location of flaws and inclusions (e. g. in castings and composites) in three-dimensional object coordinates. Therefore, and thanks to a speed-up of the measurement, CT is now routinely considered for in-line inspection of electronics, castings and composites. When precision and not speed is important, Micro-CT (μCT) can be employed for Dimensional Measurements (DM, e. g. quality assurance and shape verification), as well as for in situ testing, and for characterizing micro-structures in metals and composites. Using appropriate image processing and analysis μCT can determine the local fibre orientation in composites, the granular morphology of battery cathodes or the inter-connectivity of certain phases in casting alloys.Today, the large variety of X-ray instruments and methods poses an application problem which requires experience and a lot of knowledge for deciding which technique applies best to the task at hand. Application-specific guidelines exist for X-ray radiography testing (RT) only, whereas standardization has been applied to CT, unfortunately leaving out high resolution subμ CT, and nano-CT. For the latter exist an equally high number of NDT applications, however these instruments still necessitate a profound expertise. The task is to identify key industrial applications and push CT from system standardization to application specific automation.
Current testing methods are capable of measuring strain near the surface on structural parts, for example by using strain gauges. However, stress peaks often occur within the material and can only be approximated. An alternative strain measurement incorporates fibre-optical strain sensors (Fiber Bragg Gratings, FBG) which are able to determine strains within the material. The principle has already been verified by using embedded FBGs in tensile specimens. The transition area between fibre and aluminium, however, is not yet properly investigated. Therefore, strains in tensile specimens containing FBGs were measured by neutron diffraction in gauge volumes of two different sizes around the Bragg grating. As a result, it is possible to identify and decouple elastic and plastic strains affecting the FBGs and to transfer the findings into a fully descriptive FE-model of the strain transition area.We thus accomplished closing the gap between the external load and internal straining obtained from cast-in FBG and generating valuable information about the mechanisms within the strain transition area.It was found that the porosity within the casting has a significant impact on the stiffness of the tensile specimen, the generation of excess microscopic tensions and thus the formation of permanent plastic strains, which are well recognized by the FBG. The knowledge that FBG as internal strain sensors function just as well as common external strain sensors will now allow for the application of FBG in actual structural parts and measurements under real load conditions. In the future, applications for long-term monitoring of cast parts will also be enabled and are currently under development.
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