The separation of ethanol-water mixture is employed in the present work to produce pure ethanol, the present investigation on the separation of water from the ethanol to achieve pure ethanol by adsorption process. The different parameters like quantity of adsorbent, flow rate of feed mixture, and different adsorbents which are zeolite 3A, zeolite 4A, and silica gel are selected to study purification of ethanol by adsorption. The effect of process parameter for purification is also recorded and studied to evaluate the performance of adsorption equipment and adsorbent. The experiments are conducted at 30°C. The feed mixture is 95.6% (v/v) concentration of ethanol and 4.4% (v/v) of water. The designed adsorption column is suitable for purification of ethanol. The highest ethanol concentration 99.9443% obtained at 20 ml/min flow rate of feed mixture using 50 g of zeolite.
AA2014-T6 is an Al-Cu-Mg-based precipitation-hardened aluminium alloy widely used in aerospace due to its high strength to weight ratio. This alloy is joined by a pulsed cold metal transfer (PCMT) arc welding process to overcome the high heat input related problems in gas metal arc welding (GMAW) such as a coarser dendritic structure in the fusion zone (FZ), wider heat affected zone (HAZ), solidification and HAZ liquation cracking, softening in HAZ, and poor corrosion resistance of welded joints in salt environment. The joints were subjected to PWHT of artificial aging (AA), solution treatment (ST), and solution treatment + aging (STA) conditions. The corrosion rate was determined using a potentiodynamic corrosion test in a solution of 3.56 wt.% NaCl with pH values of 4, 7, and 11. Results disclosed that the PCMT joints subjected to the potentiodynamic corrosion test in NaCl solution of pH-4, pH-7, and pH-11 disclosed very low, moderate, and extremely high pitting corrosion, respectively. The corrosion resistance of ST joints was improved by 53.34%, 15%, and 15.12% in pH-4, pH-7, and pH-11 NaCl solution compared to as-welded joints. The pitting potential of ST joints is comparable to BM. The BM showed the pitting potential of −175, −450, and −550 mV in pH-4, pH-7, and pH-11 NaCl solution. The ST joints showed 75.29%, 29.16%, and 27.85% lower corrosion potential compared to STA joints in pH-4, pH-7, and pH-11 NaCl solution, respectively. The ST joints disclosed the lower pitting potential of −105, −425, and −505 mV in pH-4, pH-7, and pH-11 NaCl solution, respectively, whereas the STA joints revealed greater pitting potential of −425, −600, and −700 mV in pH-4, pH-7, and pH-11 NaCl solution, respectively. The superior corrosion resistance of ST joints compared to AA and STA joints is attributed to the dissolution of precipitates in Al solid solution resulting in a lower potential difference in FZ. This minimizes the preferential sites for pitting corrosion to occur.
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