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In the direct quenching and partitioning (DQ&P) process, tough ultra-high-strength steel is made by combining thermomechanical processing with quenching and partitioning to obtain martensite toughened by thin films of retained austenite. The hot rolling stage with deformation and recrystallization between the rolling passes affects the state of the austenite before quenching and partitioning. This paper describes the static recrystallization kinetics of two steels with compositions suited to DQ&P processing, viz. (in wt.%) 0.3C-1Si-2Mn-1Cr and 0.25C-1.5Si-3Mn. The stress relaxation technique on a Gleeble thermomechanical simulator provided recrystallization times over a wide range of temperature, strain, strain rate and initial grain size. The higher levels of Si and Mn made the recrystallization kinetics less sensitive to strain, strain rate and temperature. The equations derived to describe the recrystallization kinetics can be used in the design of the rough rolling part of thermomechanical processing.

A new experimental steel containing in weight percent 0.3C-2.0Mn-0.5Si-1.0Al-2.2Cr and 0.3C-1.9Mn-1.0Si-1.0Cr was hot rolled in a laboratory rolling mill and directly quenched within the martensite start and finish temperature range. It was then partitioned without reheating during slow furnace cooling to achieve tensile yield strengths over 1100 MPa with good combinations of strength, ductility and impact toughness. Gleeble thermomechanical simulations led to the selection of the partitioning at the temperatures 175 and 225 °C, which produced the desired microstructures of lath martensite with finely divided retained austenite in fractions of 6.5% and 10% respectively. The microstructures were analyzed using light and scanning electron microscopy in combination with electron backscatter diffraction and X-ray diffraction analysis. The mechanical properties were characterized extensively using hardness, tensile and Charpy V impact testing. In tensile testing a transformation induced plasticity mechanism was shown to operate with the less stable, carbon-poorer retained austenite, which transformed to martensite during straining. The auspicious results in respect to microstructures and mechanical properties indicate that there are possibilities for developing tough ductile structural steels through thermomechanical rolling followed by the direct quenching and partitioning route.

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