The article presents the results of tests carried out on the manufactured composite materials based on a two-phase NiAl/Ni 3 Al matrix, which was enriched with the addition of TiB 2 ceramic particles added in an amount of 4 and 7 vol%. The resulting mixtures were sintered by the High Pressure High Temperature (HP-HT) process. The results were compared to the results obtained for the sole matrix material produced under the same conditions. It has been shown that, at a lower density, the addition of reinforcing particles increases the composite hardness, Young's modulus and resistance to frictional wear. However, higher addition of TiB 2 (7 vol%) was observed to yield less satisfactory results, and despite higher hardness and lower density caused a decrease in other properties tested. The produced materials were characterized by a compact and highly differentiated microstructure free from any noticeable cracks and pores.
In this study, four composites with different ZrB2 content were made by the Spark Plasma Sintering (SPS/FAST) technique. The sintering process was carried out at 1373 K for 5 min under an argon atmosphere. The effect of ZrB2 reinforcing phase content on the density, microstructure, and mechanical and tribological properties of composites was investigated. The results were compared with experimental data obtained for 316L austenitic stainless steel without the reinforcing phase. The results showed that the ZrB2 content significantly affected the tested properties. With the increasing content of the ZrB2 reinforcing phase, there was an increase in the Young’s modulus and hardness and an improvement in the abrasive wear resistance of sintered composites. In all composites, new fine precipitates were formed and distributed in the steel matrix and along the grain boundaries. Microstructural analysis (Scanning Electron Microscopy (SEM), Wavelength Dispersive Spectroscopy (WDS)) has revealed that the fine precipitates chromium contained chromium as well as boron.
Samples made of AISI 316L stainless steel reinforced with 8 vol.% TiB2 particles were prepared using the high pressure-high temperature (HP-HT) method. Next, the composites were annealed at a temperature of 1200°C for different holding times. The influence of the annealing temperature and time on the properties and microstructure of AISI316L+8% vol.TiB2 composites was investigated. The structural studies showed the formation of phases containing chromium, molybdenum and boron.
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