The secondary electron emission flux in a scanning electron microscope is a powerful tool for delineation of electrically active dopant concentration, built-in potentials, and surface electric fields in semiconductor junctions. In all the secondary electron images of p-n junctions, the p-doped regions appear brighter than n-doped regions. We present a theory for the doping contrast in p-n junctions that is based on the secondary electron emission yield and surface band bending extracted from Kelvin probe force microscopy measurements. We show that the contrast is governed by the secondary electron escape depth, and their escape probability which is related to the secondary electron energy distribution and the effective electron affinity. It is found that the escape depth is the main factor determining the dopant contrast, and the escape probability has a smaller effect. In addition, our theory explains the logarithmic dependence of the measured contrast on the acceptor concentration in silicon reported by many groups.
We describe a microcantilever calorimeter consisting of an array of ten cantilevers. Each single cantilever is capable of detecting heat energy with the resolution of 50 nW Hz (Ϫ0.5) . The device is based on a Si microcantilever coated with a 1 m thick layer of SiO 2 deposited with a 700 nm thick layer of aluminum which forms a resistive microheater. Heat fluxes are monitored by detecting the cantilever deflection ͑bending͒ due to the bimaterial structure of the cantilever ͑dissimilar thermal expansion properties of SiO 2 and Al͒. The resistive microheater serves for calibration of the heat flux and for temperature sensing. In our design a piezoresistive Wheatstone bridge detector is applied for measurements of the cantilever beam deflection. The cantilever displacement detection system enables investigations in ultrahigh vacuum and low temperature conditions. The microcantilevers are manufactured in a one-dimensional array having ten individual microcantilevers which is the first step in the fabrication of an infrared detector array with spatial resolution. The displacement sensitivity versus temperature change of the described sensor array as a function of temperature change is of about 2 nm/K and an estimated resolution limit of temperature detection is Ϸ10 Ϫ3 K at 300 K. In order to demonstrate the cantilever bending sensitivity we employ the piezoresistive cantilever array as a picogram microbalance.
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