The big relevance is acquired by issues of development of methods of receiving phosphors, and studying influence on their spectral characteristics of features of structure. Red phosphors which part compounds of europium are of particular interest. Ions of europium have such properties as rather big difference of energy between its resonant and the main levels, providing radiation in the visible range; not degeneracy of these levels; the most important transitions are poorly subject to effect of the crystal field; a good possibility of the theoretical description of the processes happening in the materials containing europium ions. Ranges of a luminescence of the system received by continuous joint sedimentation of hydroxides (CDH) of europium and aluminum at a stage of crystallization of amorphous products are measured. The complex research of the CDH system is conducted by methods of the physicochemical analysis: differential and thermal, IK-spectroscopic, X-ray phase, X-ray fluorescent, power dispersive. The dependence of intensity of a luminescence of a system, from synthesis conditions is analyzed: concentration of initial components, structures of firm phases, temperatures, time (after a year of aging).
The seed shell of soybeans performs a protective function and participates in the vital processes of the seed. Soybean seeds are characterized by a unique chemical composition. The priority direction in the development of technologies for the production of foodstuffs from soybeans is the control of the quality indicators of their seeds shells. The use of a spectrofluorimeter and an IR-Fourier spectrometer allows you to study the coating material of soybean quickly and without destruction. For the purposes of comparative spectral characterization, studies were carried out on the soybean seed envelope of the untreated and treated modifier mixture. Main characteristics of luminescence excitation spectrum are determined including recording wavelength, excitation spectrum region, excitation wavelength intensity. Parameters glow attenuation are revealed by spectral-kinetic studies of phosphorescence of soybean seeds shell. IR spectroscopic analysis of milled and whole soybean seeds, as well as modifiers, allows us to interpret groupings that have characteristic oscillation frequencies. The main spectral characteristics of the soybean seed shell are determined, including wave numbers, incident radiation wavelength, transmission, and oscillation character. Modifiers adsorbed on surface of soybean seed shell are identified. The type of adsorption of the modifier shell is defined.
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