A smartphone application, called CAnal, was developed as a colorimetric analyzer in paper-based devices for sensitive and selective determination of mercury(II) in water samples. Measurement on the double layer of a microfluidic paper-based analytical device (μPAD) fabricated by alkyl ketene dimer (AKD)-inkjet printing technique with special design doped with unmodified silver nanoparticles (AgNPs) onto the detection zones was performed by monitoring the gray intensity in the blue channel of AgNPs, which disintegrated when exposed to mercury(II) on μPAD. Under the optimized conditions, the developed approach showed high sensitivity, low limit of detection (0.003 mg L-1 , 3SD blank/slope of the calibration curve), small sample volume uptake (two times of 2 μL), and short analysis time. The linearity range of this technique ranged from 0.01 to 10 mg L-1 (r 2 = 0.993). Furthermore, practical analysis of various water samples was also demonstrated to have acceptable performance that was in agreement with the data from cold vapor atomic absorption spectrophotometry (CV-AAS), a conventional method. The proposed technique allows for a rapid, simple (instant report of the final mercury(II) concentration in water samples via smartphone display), sensitive, selective, and on-site analysis with high sample throughput (48 samples h-1 , n = 3) of trace mercury(II) in water samples, which is suitable for end users who are unskilled in analyzing mercury(II) in water samples.
In this work we present a full-passive flexible multigas sensing tag for the determination of oxygen, carbon dioxide, ammonia, and relative humidity readable by a smartphone. This tag is based on near field communication (NFC) technology for energy harvesting and data transmission to a smartphone. The gas sensors show an optic response that is read through high-resolution digital color detectors. A white LED is used as the common optical excitation source for all the sensors. Only a reduced electronics with very low power consumption is required for the reading of the optical responses and data transmission to a remote user. An application for the Android operating system has been developed for the power supplying and data reception from the tag. The responses of the sensors have been calibrated and fitted to simple functions, allowing a fast prediction of the gases concentration. Cross-sensitivity has also been evaluated, finding that in most of the cases it is negligible or easily correctable using the rest of the readings. The election of the target gases has been due to their importance in the monitoring of modified atmosphere packaging. The resolutions and limits of detection measured are suitable for such kinds of applications.
Here we present a fast and cheap prototyping technique for the realisation of paper-based microfluidic devices simply by using a stamp and indelible ink. The proposed mechanism involves contact stamping of indelible ink to laboratory filter paper using a PDMS stamp, which defines the microfluidic structure. It is a cleanroom and washing steps-free method which provides a reproducible method for the production of functional paper-based microfluidic devices in a single step in less than 10 s. The method is fully characterised and the concept has been applied, as a proof-of-principle, for the realisation of a low-cost colorimetric glucose sensor.
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