An efficient preparative method was developed for the synthesis of previously unreported fullerenylstyrenes based on the reaction of C 60 fullerene with terminal acetylenes and EtMgBr in the presence of Ti(Oi-Pr) 4 . The voltammetric curves of the prepared fullerenylstyrenes were studied, and good prospects for their application as acceptor materials for bulk heterojunction solar cell were demonstrated.
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