In the aerospace industry, materials used as modern engine components must be able to withstand extreme operating temperatures, creep, fatigue crack growth and translational movements of parts at high speed. Therefore, the parts produced must be lightweight and have good elevated-temperature strength, fatigue, resistant to chemical degradation, wear and oxidation resistance. High entropy alloys (HEAs) characterize the cutting edge of high-performance materials. These alloys are materials with complex compositions of multiple elements and striking characteristics in contrast to conventional alloys; their high configuration entropy mixing is more stable at elevated temperatures. This attribute allows suitable alloying elements to increase the properties of the materials based on four core effects , which gives tremendous possibilities as potential structural materials in jet engine applications. Researchers fabricate most of these materials using formative manufacturing technologies; arc melting. However, the challenges of heating the elements together have the tendency to form hypoeutectic that separates itself from the rest of the elements and defects reported are introduced during the casting process. Nevertheless, Laser Engineering Net Shaping (LENS™) and Selective Laser Melting (SLM); a powderbased laser additive manufacturing process offers versatility, accuracy in geometry and fabrication of three-dimensional dense structures layer by layer avoiding production errors.
The heating and cooling profiles experienced during laser additive manufacturing results in residual stresses build up in the component. Therefore, it is necessary to perform post build stress relieving towards the retention and improvement of the mechanical properties. However the thermal treatments for conventional manufacturing do not seem to completely accommodate these rapid heating and cooling cycles of laser processing techniques such as powder bed fusion. Characterizations such as density measurements on the samples were performed employing the Archimedes principle; hardness testing was performed on the Zwick micro/macro (Hv) hardness tester, SEM and Electron backscatter diffraction (EBSD). Fracture toughness and crack growth was conducted on a fatigue crack machine. All characterization was done after stress relieving of Selective Laser Melting (SLM) produced samples at 300 °C for 2 hrs was performed in a furnace. The mechanical properties appear to be rather compromised instead of being enhanced desirably. As-built SLM produced tensile specimens built in different directions exhibited significantly favorable mechanical properties. However, post stress relieve thermal treatment technique deteriorated the strength while increasing the ductility significantly. Nonetheless, fatigue crack growth and fracture toughness illustrated positive outcome in terms of fatigue life on SLM produced AlSi10Mg components in application.
Aerospace components and their coatings are required to possess excellent surface properties over a wide temperature range. Stainless steels, titanium, nickel superalloy, and more recently high entropy alloys (HEAs) have been used to improve the exterior properties of these components. In this study, AlTiCrFe-CoNi and AlCoCrFeNiCu HEAs were successfully fabricated using laser additive manufacturing to produce coatings on an A301 steel base plate. The influence of the laser parameters (laser power and scan speed) on the microstructure and hardness properties were also investigated. The results revealed that coatings homogeneously adhered to the baseplate. The optimum processing parameters for both alloys with defect-free structures at a preheat temperature of 400 • C, were at 1200-1600 W at 8-12 mm/s with the layers composed of both face centred-cubic (FCC) and body centred-cubic (BCC) phases. The laser parameters affected the quality and hardness properties of the alloys. The results showed that optimizing the laser parameters achieved by preheating temperature invariably improved the performance of the alloys with potential coatings and structural applications.
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