Structural changes (martensitic transformation, rearrangements of martensitic variants) in shape memory alloys have an intermittent character that is accompanied by the emission of different (thermal, acoustic, and magnetic) noises, which are fingerprints of the driven criticality, resulting in a damped power-law behaviour. We will illustrate what kinds of important information can be obtained on the structural changes in shape memory alloys. It was established that the power exponents of distributions of acoustic emission (AE) parameters (energy, amplitude, etc.), belonging to martensitic transformations, show quite a universal character and depend only on the symmetry of the martensite. However, we have shown that the asymmetry of the transformation (the exponents are different for the forward and reverse transformations) results in as large differences as those due to the martensite symmetry. We will also demonstrate how the recently introduced AE clustering method can help to identify the different contributions responsible for the asymmetry. The usefulness of the investigations of time correlations between the subsequent events and correlations between acoustic and magnetic noise events in ferromagnetic shape memory alloys will be demonstrated too. Finally, examples of acoustic and magnetic emissions during variant rearrangements (superplastic or superelastic behaviour) in the martensitic state will be described.
Simultaneous differential scanning calorimetry, DSC, and acoustic emission, AE, measurements were carried out for single crystals of quenched and stress-induced martensite stabilized (SIM-aged) shape memory Ni51Fe18Ga27Co4 alloy. The transformation temperatures were shifted to higher values, the forward (from austenite to martensite) and reverse transitions became sharper and the width of the hysteresis increased in the SIM-aged sample. The energy distributions of acoustic hits showed similar behaviour to those of the quenched sample and the energy exponents, characterizing the power law behaviour, were also similar. For SIM-aged alloys at heating, in accordance with the sharper (burst-like) transition observed in the DSC run, few high-energy solitary hits were observed, and these hits did not fit to the energy distribution function fitted for smaller energies. Thus, these high-energy events were attributed to high sudden jumps in the phase transition during heating. The effect of long-range order (by applying a heat treatment at 573 K for 6 h to transform the B2 austenite to ordered L21 structure) and the SIM-aging on the transformation entropy was also investigated by DSC. It was found that the entropy was about 36% smaller after SIM-aging of the quenched sample and it was practically unchanged after austenite stabilization.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.