In the present investigation, thin sheets of stabilized and unstabilized ferritic stainless steel were welded in butt joint configuration using irradiation of a 1070 nm fiber-laser. Using optical microscopy, the microstructural evolution upon alternating heat input was characterized. In addition to that, hardness and tensile tests were carried out on the specimens. Detailed focus was given to the intergranular corrosion properties, which were investigated on basis of the Strauss test with different times of exposure to the corrosive environment. Following these tests, the mechanical properties of the joints were characterized using tensile tests. A combination of the latter with an inspection by μ-CT analysis allows for the proposition of an intergranular corrosion rate with regard to the degradation of the joint strength.
A Co-Ni-Ga high-temperature shape memory alloy has been additively manufactured by directed energy deposition. Due to the highly anisotropic microstructure, i.e. columnar grains featuring a strong near-001 texture in build direction, the as-built material is characterized by a very low degree of constraints and, thus, shows excellent superelasticity without conducting a post-process heat treatment. As characterized by in situ deformation testing and post-mortem microstructural analysis, additive manufacturing employing directed energy deposition seems to be highly promising for processing of shape memory alloys, which often suffer difficult workability. IMPACT STATEMENTThe present work establishes a new pathway towards realization of high performance shape memory alloys by additive manufacturing and, thus, will stimulate further research in this field directed towards application.
In the present study, compositionally-graded structures of AISI 316L and CoCrMo alloy are manufactured by powder-based laser-beam directed energy deposition (DED-LB). Through a process-integrated adjustment of powder flow, in situ alloying of the two materials becomes feasible. Thus, a sharp and a smooth transition with a mixture of both alloys can be realized. In order to investigate the phase formation during in situ alloying, a simulation approach considering equilibrium calculations is employed. The findings reveal that a precise compositional as well as functional gradation of the two alloys is possible. Thereby, the chemical composition can be directly correlated with the specimen hardness. Moreover, phases, which are identified by equilibrium calculations, can also be observed experimentally using scanning electron microscopy (SEM) and energy-dispersive X-ray-spectroscopy (EDS). Electron backscatter diffraction (EBSD) reveals epitaxial grain growth across the sharp transition region with a pronounced <001>-texture, while the smooth transition acts as nucleus for the growth of new grains with <101>-orientation. In light of envisaged applications in the biomedical sector, the present investigation demonstrates the high potential of an AISI 316L/CoCrMo alloy material combination.
Laser-based Directed Energy Deposition (DED-LB) represents a production method of growing importance for cladding and additive manufacturing through the use of metal powders. Yet, most studies utilize substrate materials with thicknesses of multiple millimeters, for which laser cladding of thin-sheet substrates with thicknesses less than 1 mm have only been scarcely studied in the literature. Most studies cover the use of pulsed laser sources, since sheet distortion due to excess energy input is a key problem in laser cladding of thin-sheet substrates. Hence, the authors of the present investigation seek to expand the boundaries of cladding thin-sheet substrates through the use of a high-speed laser cladding approach which utilizes a continuous-wave, ytterbium fiber laser and traverse speeds of 90 mms−1 to clad stainless steel sheets with a thickness of 0.8mm. Furthermore, fundamental process–property relationships for the target values of clad width, clad height, and dilution depth are studied and thoroughly discussed. Additionally, process maps for the target values are established based on manifold experiments, and the significance of process parameters on target values is studied using analysis of variance. The results demonstrate that clad widths as high as 1413 μm and dilution depths as low as 144 μm can be obtained by high-speed laser cladding of thin-sheet substrates. Thus, pathways toward thin-sheet substrates with enhanced performance are opened.
In the present investigation, thin sheet geometries of commercially pure titanium (cp, grade 4) are butt-welded to AISI 316L stainless steel as well as Nitinol by means of micro electron beam welding using filler materials. In order to avoid mixing of the base materials, the refractory metals tantalum, niobium and hafnium are applied as intermediate layers. Owing to the biocompatibility of these filler materials, the final products are suitable for medical technology applications. In combination with low energy inputs and precise beam alignments, it is demonstrated that high-quality and crack-free joints can be produced using micro electron beam welding. The welded joints are analysed using nanoindentation to identify critical weld areas, e.g. high concentrations of intermetallic compounds, and to evaluate the compatibility of the base and filler materials. To correlate the hardness mappings with the microstructural evolution of the welds, an exemplary joint is analysed by means of electron backscatter diffraction and energy dispersive X-ray spectroscopy with special emphasis on intermixing and the formation of intermetallic compounds. Based on the generated hardness mappings as well as the ultimate tensile strengths of the joints, it will be concluded which filler material provides the most promising results for the given material combinations.
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