In this study, oil extraction from Niger seeds was evaluated with different microwave irradiation times (0–200 s) and pulsed electric fields (PEF) intensities (0–5 kV/cm) as pretreatments. Then, oil extraction was completed with a screw press at different rotation speeds (11–57 rpm). Quality parameters including extraction efficiency, acidity and peroxide values (PVs), chlorophyll, and phenolic contents along with fatty acid profiles and tocopherol levels of the extracted oils were determined as responses. With enhancements in microwave time, PEF intensity and press rotation, the chlorophyll contents, acidity/PVs, and total phenolics of oils increased similar to oil extraction efficiency although it was reduced later. The optimized conditions selected by response surface methodology were determined as 156.23 s, 1.18 kV/cm, and 20 rpm for microwave time, PEF intensity and press speed, respectively. Fatty acid analysis revealed that linoleic acid was the most predominant fatty acid in the extracted oil. Application of the mentioned pretreatments may lead to a reduction in unsaturated fatty acids and escalation of saturated ones (p < .05). High‐performance liquid chromatography results indicated that α‐tocopherols are the most common tocopherols in Niger seed oil and microwave‐PEF pretreatments may lead to 2.79% increase in tocopherols content.
In this study, optimization of the extraction of canola seeds oil was investigated using microwave-pulsed electric field seeds pretreatment (MW-PEF) with different MW times (0 to 200 s) and PEF intensities (0 to 5 kV/cm). The seeds oil was then extracted using screw press with different speeds (11 to 57 rpm). Oil extraction efficiency, refractive index, peroxide and phenolic compounds of oil and meal protein were measured. Tocopherols content of the best sample was also measured. The results showed that the peroxide and phenolic compounds increased at higher time, intensity and speed. An increase in the MW time and PEF intensity at first led to an increase in the oil extraction efficiency and meal protein but then both parameters decreased. The efficiency of oil extraction and protein decreased at higher speeds. The refractive index of all samples was 1.475. Gamma tocopherol was predominate one in canola oil and applying the pretreatment led to an increase in the number of total tocopherols. Treating at 1.28 kV/cm for 140.5 s and 28.71 rpm was chosen as the optimum condition with high desirability (0.744).
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