Commercial flakes of graphite were prepared into functionalized graphene oxide (GO) by chemical treatment. After the exfoliation and intercalation of graphene into functionalized graphene oxide that formed stable colloidal dispersion in polar aprotic solvent, the reduction process was undertaken by continuous stirring with hydrazine hydrate. The reduced material was characterized by X-ray diffraction (XRD), attenuated total reflectance (ATR) FT-IR, ultraviolet visible (UV-vis), atomic force microscopy (AFM) and Raman spectroscopy which confirm the oxidation of graphite and reduction of graphene oxide into graphene sheet.
It is universally known that the preparation of high quality graphene on a large scale and in a cost-effective manner is essential for many technological applications. Graphene oxide (GO) has emerged as the precursor of choice for bulk production of graphene-based materials, as it can be synthesized from inexpensive graphite powders. In this paper, a simple method is described for reduction of GO solution by a free and green irradiation based technique. The majority of oxygencontaining functional groups of GO are removed by sun light. This methodology provides an effective way to quantitatively produce high quality graphene sheets. This paper presents irradiation by sun light of synthesized graphene oxide nano-flakes prepared by Hummer's method. These nano-flakes have been successfully reduced while the dynamic of this irradiation process is discussed. The irradiated nano-flakes of graphene oxide have been investigated using X-Ray diffraction, ATR-FTIR and UV-Vis-NIR.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.