The phase equilibriums in the FeGa 2 S 4 -FeIn 2 S 4 and FeS-FeIn 2 S 4 systems were experimentally investigated by means of differential thermal and X-ray diffraction analyses. It found that they are quasi-binary and characterized by limited mutual solubility of starting compounds. The phase with composition FeGaInS 4 crystallizes in the FeGa 2 S 4 -type structure, melts at 1375 K without decomposition, and can be characterized as a congruently melting compound by its beh avior in the phase diagram.
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