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Melamine formaldehyde composites have been synthesized with chlorides and micro- and nanoparticles of transition metals (Co, Ni, Cu) entered into polymer during the polycondensation of melamine with formaldehyde. The received composites were studied by the X-ray diffraction and scanning electronic microscopy and applied as catalysts to cathode activation in cyclohexanone electrohydrogenation. For composites of MF+MCl2 it was established higher catalytic activity than for МF+М0.