27Al NMR studies of the Y3—xYbxAl5O12 mixed garnets were performed. The magnetic moment of Yb3+ ions in the garnets was determined. The quadrupole coupling constants were calculated for Al in a‐ and d‐positions. It was shown that the mixed garnets with x = 0.75 and 1.00 should be treated as partially ordered solid solutions. A model of substitutional ordering for these mixed garnets was suggested.
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