Small fatigue crack propagation in bimodal harmonic structured titanium alloy (Ti-6Al-4V) with high strength and ductility was examined under four-point bending at a stress ratio of 0.1 in the ambient laboratory atmosphere. The crack profiles were observed using optical microscopy and scanning electron microscopy, and analyzed using an electron backscattered diffraction to examine the mechanism of small fatigue crack propagation. Fatigue crack paths were not influenced by the bimodal harmonic structure, and the crack growth rates, da/dN, in the harmonic structured Ti-6Al-4V were almost the same as those in a material with coarse acicular microstructure for comparable values of stress intensity range, K. In contrast, the harmonic structured Ti-6Al-4V had a higher resistance of fatigue crack initiation due to the grain refinement induced by mechanical milling, which resulted in an increase of the fatigue life and fatigue limit. Furthermore, the statistical fatigue properties of Ti-6Al-4V alloy were analyzed using the stress dependence of Weibull parameters to quantitatively examine the effects of the bimodal harmonic structure on its fatigue life.
To examine near-threshold fatigue crack propagation in commercially pure (CP) titanium with a bimodal harmonic structure, which is defined as a coarse grained structure surrounded by a network of fine grains, K-decreasing tests were conducted. The crack growth rates for harmonic-structured CP titanium were higher than those for homogeneous material with coarse grains at comparable stress intensity range, while the threshold stress intensity range was lower. This phenomenon was attributed to a reduction in the extent of crack closure and the effective threshold stress intensity range, resulting from the presence of fine grains in the harmonic structure.
This study aimed at investigating the influence of microstructure on mechanical properties of Harmonic Structured (HS) pure-Ni compacts. The harmonic structure is a heterogeneous microstructure with a spatial distribution of fine grains (FG) and coarse grains (CG), that is, the CG areas ('Core') embedded in the matrix of three-dimensionally continuously connected network of FG areas ('Shell'). The HS pure-Ni samples were fabricated by powder metallurgy route consisting of mechanical milling (MM) of plasma rotated electrode processed pure-Ni powder and subsequent sintering by Spark Plasma Sintering. The plastic deformation at powder particle surface increases with increasing MM time. As a result, after sintering, shell fraction also increases in the HS pure-Ni samples. It was found that the fraction of a "shell" area is an important parameter controlling the balance of the mechanical properties of the HS pure-Ni compacts. The HS pure-Ni with a higher fraction of "shell" area demonstrated higher strength and approximately similar elongation as compared to the homo Ni samples and HS pure-Ni samples containing low shell fraction. Moreover, the effects of strain hardening rates and strain hardening exponents on deformation behaviour of HS pure-Ni samples were also discussed.
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