The distribution characteristics of in-grain misorientation axes (IGMA) in cold-rolled pure titanium were investigated using electron backscatter diffraction (EBSD). Depending on the orientation of individual grains, two distinct IGMA distribution patterns were observed: one with strong intensities of IGMA around h0001i and the other with those around huvt0i. Analyses based on the Taylor axes and Schmid factors of possible slip modes suggested that the former pattern arises from predominant activation of prism hai slip, while activation of f11 " 22gh " 1 " 123i slip under the suppression of prism hai slip results in the latter pattern. It was also found that prism hai slip becomes more active with increasing strain, playing a critical role in the plasticity of pure titanium. The present work demonstrates that IGMA analysis of EBSD data may be used to explore the active slip mode in polycrystalline hexagonal-close-packed (hcp) metals deformed to moderate to large strains.
The effect of sample orientation on the mechanical properties of commercially pure (CP) titanium plate with a transverse split basal texture was investigated at room temperature (RT) using plane strain compression (PSC). A large variation in flow stress of up to~60 pct was found for samples of different orientations. The major sources of this variation were revealed by measuring area fractions for individual twin modes using electron backscatter diffraction (EBSD) and calculating Schmid factors for all important slip and twinning modes. Importantly, the Schmid factors were calculated for all orientations in Euler space because there are significant variations over all orientations for the PSC stress state, unlike uniaxial compression or tension. The Schmid factor analysis and twin data for the wide variety of orientations tested enabled the conclusion to be drawn reliably that higher flow stresses were primarily due to an unfavourable orientation for prism-a h i slip. A greater proportion of 11 " 22 È É to 10 " 12 È É twinning was also a major factor in the higher flow stresses. Increased strain hardening was observed in the sample orientation that showed a dramatic texture change to a more difficult orientation for further deformation as a result of dominant 10 " 12 È É twinning. This indicated that reorientation hardening was the responsible mechanism.
This paper investigates the changes in deformation mechanisms of commercially pure
titanium over a range of temperatures for different orientations relative to the initial rolling texture.
Samples from grade 1 titanium plate were tested in plane strain compression (PSC). Extremes of
orientation relative to the predominant split basal texture were tested at temperatures from 25°C to
700°C. Specimens were subsequently examined using X-ray texture analysis and electron
back-scatter diffraction (EBSD). Changing the orientation resulted in substantial yield stress
anisotropy. This was found to be largely related to the orientation of the dominant texture relative to
the most favorable orientation for the easiest slip mode (prism slip), and significantly but to a lesser
extent on differences in twinning behaviour. The most important difference in twinning was the
operation of {1012} tensile twinning in c-axis tension and {1122} compression twinning in c-axis
extension. Calculations indicated that at low temperature both of these twinning modes accommodate
a significant amount of strain. Twinning was also found to be the most significant factor affecting
work hardening behaviour, with reorientation hardening occurring for some sample orientations. As
temperature was increased above ~350°C {1011} twinning became the dominant twinning mode, but
its contribution to the strain was not as large as the low temperature twinning modes, and the total
amount of twinning decreased with temperature. The decrease in twinning with increasing
temperature led to a reduction in the difference in work hardening behaviour. The quantitative
information gathered in the course of this work is discussed in the context of mechanical property
prediction.
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