Use of microwave radiation in extraction
of natural products is
increasing in an exponential manner because of its inherent greener
features. The extraction of essential oil from the leaves of lemongrass
was carried out using microwave radiation and compared with hydrodistillation.
The process was optimized using the Taguchi method, and the highest
yield was obtained at a 200 mL volume of water, 30 min of rehydration
time, and 45 min of extraction time. The extraction time was found
to be the most influential parameter affecting the process. A data
fit for kinetic desorption models was carried out. The biological
activities of the lemongrass oil were also assessed. A microscopic
study was performed to understand the extraction mechanism. A comparison
showed that microwave-assisted extraction is a better alternative
to hydrodistillation in terms of yield, extraction time, biological
activity, energy efficiency and environmental friendliness.
A novel technique for the extraction of citral from the
leaves
of Cymbopogon flexuosus (Steud.) Wats.
using hydrotropic solutions (sodium salicylate and sodium cumene sulfonate)
was investigated. The yield of citral was dependent on the concentration
of hydrotrope, solid loading, temperature, and size of the plant material.
Using the Taguchi method, the extraction was optimized, and both the
hydrotropes gave the highest yield of citral at a concentration of
1.75 M, 5% solid loading, a temperature of 30 °C, and a size
of 0.25 mm of the plant material. Sodium salicylate gave a better
extraction yield of citral than sodium cumene sulfonate. The microscopic
analysis of plant leaves provided insight into the extraction mechanism.
A kinetic study was carried out to check the extraction efficiency
for both the hydrotropes. The hydrotropic solution was successfully
recycled. Using hydrotropic extraction, citral could be extracted
under normal operating conditions, and the use of traditional organic
solvents could be eliminated. As a simple and environmentally friendly
technique, hydrotropic extraction could be utilized for the extraction
of bioactive compounds from plants.
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