Residence-time distribution (RTD) experiments were performed to analyze an industrial scale three-tube series continuous pulping digester’s hydrodynamic performance. An impulse of radiotracer 82Br (γ energy source) was introduced at the inlet of the first tube. The radiotracer concentration in the liquid phase was traced at the outlet of each tube. The input behavior of the radiotracer converted to a non-ideal pulse tracer input for the second and third tubes of the digester. Numerical convolution is adopted to deal with the non-ideal pulse input of the radiotracer. A modeling procedure for determining the RTD from the outlet tracer concentration data is proposed. A plug flow component followed by axial dispersion model is considered, and is adjusted after its convolution with the inlet tracer concentration data to obtain the RTD of the individual tubes. The obtained RTD data are analyzed to explain the flow behavior, degree of dispersion, and flow abnormalities existing in the digester. The mean residence-time (MRT), and dispersion number are estimated for the model components for the three tubes. The vessel dispersion number is found to decrease from tube 1 to tube 3. Overall, the conversion of the highly dispersed flow regime into the plug-flow regime is observed in the whole digester.
Radiotracer-based residence time distribution (RTD) measurements were performed for two identical wheat straw pulping digesters to evaluate and compare their performances. The radiotracer technetium ( 99m Tc) as sodium pertechnetate was used to follow the liquid phase inside the digester. The product quality of both digesters was not identical for similar sets of operating conditions. Temperature, pressure, and mass flow rates were the influencing parameters, and the experimental and theoretical mean residence time (MRT) were compared. A significant amount of flow abnormalities was observed in the second digester as compared to the first one, including channeling, dead volume, scaling, and bypassing. The axial dispersion model and tank in series with the back-mixing model were suitable for modeling the obtained RTD data.
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