We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically-bent crystal analyzer (SBCA), and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ~5 keV to ~10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W xray tube, we find count rates for nonresonant x-ray emission spectroscopy (XES) comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For xray absorption near edge structure (XANES), the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial highpower line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10 6 -10 7 photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide or noble-metal active species.
The jovian system is of particular interest for studying magnetic induction in icy ocean worlds. Jupiter has a strong magnetic field whose dipole axis is tilted 9.6° with respect to its rotation axis (Acuna & Ness, 1976), while the orbits of the Galilean moons lie very nearly in the equatorial plane of Jupiter. This means that Jupiter's magnetic field varies in time at the orbital positions of the satellites. Also, the outer layers of the
The jovian system is of particular interest for studying magnetic induction in icy ocean worlds. Jupiter has a strong magnetic field whose dipole axis is tilted 9.6° with respect to its rotation axis (Acuna & Ness, 1976), while the orbits of the Galilean moons lie very nearly in the equatorial plane of Jupiter. This means that Jupiter's magnetic field varies in time at the orbital positions of the satellites. Also, the outer layers of the
The Galileo mission to Jupiter discovered magnetic signatures associated with hidden subsurface oceans at the moons Europa and Callisto using the phenomenon of magnetic induction. These induced magnetic fields originate from electrically conductive layers within the moons and are driven by Jupiter's strong time‐varying magnetic field. The ice giants and their moons are also ideal laboratories for magnetic induction studies. Both Uranus and Neptune have a strongly tilted magnetic axis with respect to their spin axis, creating a dynamic and strongly variable magnetic field environment at the orbits of their major moons. Although Voyager 2 visited the ice giants in the 1980s, it did not pass close enough to any of the moons to detect magnetic induction signatures. However, Voyager 2 revealed that some of these moons exhibit surface features that hint at recent geologically activity, possibly associated with subsurface oceans. Future missions to the ice giants may therefore be capable of discovering subsurface oceans, thereby adding to the family of known “ocean worlds” in our Solar System. Here, we assess magnetic induction as a technique for investigating subsurface oceans within the major moons of Uranus. Furthermore, we establish the ability to distinguish induction responses created by different interior characteristics that tie into the induction response: ocean thickness, conductivity and depth, and ionospheric conductance. The results reported here demonstrate the possibility of single‐pass ocean detection and constrained characterization within the moons of Miranda, Ariel, and Umbriel, and provide guidance for magnetometer selection and trajectory design for future missions to Uranus.
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