The effect of CaTiO3 addition on the complex permittivity of MgTiO3 powder was characterized with an open-ended coaxial cavity resonator in the range of 2.12–3.66 GHz. Permittivities and loss tangents of (1 − x)MgTiO3-xCaTiO3 composite powders with x of 0, 2, 5, and 10 mol. % were measured and compared to theoretical values. Inclusion permittivities and dielectric loss tangents were determined by using Bruggeman symmetric and Looyenga mixing rules and a general mixing model. Additions of CaTiO3 resulted in a clear increase in inclusion permittivities from 13.4 up to 14.9 and in loss tangents from 7.1 × 10−3 up to 8.5 × 10−3. Comparison with the theoretical loss tangent values and quantitative determination of CaTiO3 molar ratios by using measured loss tangents and a general mixing model gave a good correlation. The characterization method was proved to be capable of detecting dielectric changes of MgTiO3–CaTiO3 composite powder and of quantifying the amount of additional substances. This information can be exploited, for example, in the analysis and quality control of different composite powders.
An open ended coaxial cavity method for dielectric characterization of powdery substance operating at 4.5 GHz in TEM mode is presented. Classical mixing rules and electromagnetic modeling were utilized with measured effective permittivities and Q factors to determine the relative permittivity and dielectric loss tangent of different powders with εr up to 30. The modeling enabled determination of the correction factor for the simplified equation for the relative permittivity of an open ended coaxial resonator and mixing rules having the best correlation with experiments. SiO2, Al2O3, LTCC CT 2000, ZrO2, and La2O3 powders were used in the experiments. Based on the measured properties and Bruggeman symmetric and Looyenga mixing rules, the determined dielectric characteristics of the powders exhibited good correlation with values in the literature. The presented characterization method enabled the determination of dielectric properties of powdery substances within the presented range, and therefore could be applied to various research fields and applications where dielectric properties of powders need to be known and controlled.
A novel technique to periodically modulate the aperture of a coupled mode leaky coaxial cable (LCX) is presented in this communication. The surface wave (monofilar mode) over the cable is modulated by periodically slotted aperture, converting it to a leaky wave. This leaky wave due to periodic modulation complements the leaked bifilar mode, thus enhancing the radiation efficiency of the LCX. The numerical results obtained through CST simulation are presented to prove the co-existence of a complex surface wave and a leaky wave over the surface of periodically modulated cable. As a proof of concept, a periodically slotted LCX operating at 4.5 GHz is designed and fabricated. Parametric studies are performed to observe the influence of the key parameters on the radiation performance. The measured results reasonably agree with the simulations.
The effect of moisture adsorption in the characterization of dielectric powders by an indirectly coupled open-ended coaxial cavity method operating at 4.5 GHz was analyzed. SiO2, Al2O3, and ZrO2 powders were exposed to 5% and 100% relative humidity levels and Bruggeman symmetric, Looyenga, and General Mixing Model equations were used to determine changes in permittivity and loss tangent of the inclusions. Low moisture adsorption (0.1–2.5 vol. %) induced only a small change in inclusion permittivity but had a pronounced impact on dielectric losses. Calculated moisture percentages based on responses of the resonator and the General Mixing Model correlated well with traditional mass based determination. The presented characterization method exhibited high sensitivity for the determination of dielectric properties of powders and their moisture content to be further utilized in, e.g., process and quality monitoring.
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