The XRD profiles and FTIR analysis of sludge aggregates, Mg–Al layered double hydroxides, produced during electrocoagulation processes are presented. The data describes the composition of materials (LDH) produced at different operations conditions (atmospheric conditions and Mg2+/Al3+ ratio). The data show the diffraction peaks of (003), (006), (018) and (110) crystal planes for hydrotalcite structure.
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