The synthetic precursors pyridine‐2(1H)‐thiones 2a,b and bis(pyridine‐2(1H)‐thione) derivative 4, using aldehydes 1a,b incorporating 2,6‐dibromophenoxy moiety, were prepared and used to synthesize the novel target materials bis[(5‐cyanopyridin‐6‐yl)sulfanyl]butanes 5a,b, bis(2‐S‐alkylpyridines) 8a,b, and bis(3‐aminothieno[2,3‐b]pyridines) 13a–c through facile procedures. Characterization of the newly prepared compounds via elemental analyses and spectral data is established.
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