Semi-empirical total cross sections for electron scattering of noble gases (Ne, Ar and Kr) in the energy range 0.5-10 keV have been obtained by combining transmission-beam measurements for impact energies up to 6 keV with an asymptotic behaviour at higher energies according to the Born-Bethe approximation. The influence of the forward electron scattering on the experimental system has been evaluated by means of a Monte Carlo electron transport simulation. Theoretical values have also been obtained by applying the Born approximation in the case of inelastic processes and by means of an atomic scattering potential for the elastic part. The results of these calculations show an excellent agreement with the semi-empirical values in the above-mentioned energy range.
Detailed uncertainty reporting is imperative for proficiency tests and comparison exercises because uncertainties need to be comparable and trusted by all the participants. Even though participants do their best to follow the Guide to the Expression of Uncertainty in Measurement, ambiguities and divergences about uncertainty evaluation remain. Consequently, to analyze the situation, the CCRI (II) Uncertainties Working Group proposed a comparison exercise (CCRI(II)-S7) about the uncertainty evaluation of a relatively simple primary activity measurement: the standardization of a 60Co source by coincidence counting.
To be able to understand how various NMIs calculate coincidence counting uncertainties, our study focused on two of the dominant uncertainty components commonly quoted for 4πβ-γ coincidence counting in the International Reference System (SIR) submissions and Key Comparison exercises: efficiency-extrapolation and weighing. Participants from twelve different laboratories were sent the same set of measurement data from the analysis of a 60Co solution standardized at the National Physical Laboratory (NPL).
Our study demonstrated the extent of the different interpretations of the uncertainty components. Some factors causing large discrepancies were isolated and are discussed. Further studies of other techniques using a similar approach would be beneficial for the metrology community.
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To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/.The final report has been peer-reviewed and approved for publication by the CCRI, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).
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