2Graphical entry and synopsis Reactions of [8, ) 2 -nido-8,7-RhSB 9 H 10 ] (1) with PR 3 afford 11-vertex rhodathiaboranes in which the resulting ligand configuration is driven by the nature of the monodentate phosphine. The lability of some of the species is demonstrated by variable NMR studies, which give mechanistic insights on the substitutional chemistry of 11-vertex nido-rhodathiaboranes.
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