The Scanning Habitable Environments with Raman and Luminescence for Organics and Chemicals (SHERLOC) is a robotic arm-mounted instrument on NASA’s Perseverance rover. SHERLOC has two primary boresights. The Spectroscopy boresight generates spatially resolved chemical maps using fluorescence and Raman spectroscopy coupled to microscopic images (10.1 μm/pixel). The second boresight is a Wide Angle Topographic Sensor for Operations and eNgineering (WATSON); a copy of the Mars Science Laboratory (MSL) Mars Hand Lens Imager (MAHLI) that obtains color images from microscopic scales (∼13 μm/pixel) to infinity. SHERLOC Spectroscopy focuses a 40 μs pulsed deep UV neon-copper laser (248.6 nm), to a ∼100 μm spot on a target at a working distance of ∼48 mm. Fluorescence emissions from organics, and Raman scattered photons from organics and minerals, are spectrally resolved with a single diffractive grating spectrograph with a spectral range of 250 to ∼370 nm. Because the fluorescence and Raman regions are naturally separated with deep UV excitation (<250 nm), the Raman region ∼ 800 – 4000 cm−1 (250 to 273 nm) and the fluorescence region (274 to ∼370 nm) are acquired simultaneously without time gating or additional mechanisms. SHERLOC science begins by using an Autofocus Context Imager (ACI) to obtain target focus and acquire 10.1 μm/pixel greyscale images. Chemical maps of organic and mineral signatures are acquired by the orchestration of an internal scanning mirror that moves the focused laser spot across discrete points on the target surface where spectra are captured on the spectrometer detector. ACI images and chemical maps (< 100 μm/mapping pixel) will enable the first Mars in situ view of the spatial distribution and interaction between organics, minerals, and chemicals important to the assessment of potential biogenicity (containing CHNOPS). Single robotic arm placement chemical maps can cover areas up to 7x7 mm in area and, with the < 10 min acquisition time per map, larger mosaics are possible with arm movements. This microscopic view of the organic geochemistry of a target at the Perseverance field site, when combined with the other instruments, such as Mastcam-Z, PIXL, and SuperCam, will enable unprecedented analysis of geological materials for both scientific research and determination of which samples to collect and cache for Mars sample return.
Just as geological samples from Earth record the natural history of our planet, astromaterials hold the natural history of our solar system and beyond. Astromaterials acquisition and curation practices have direct consequences on the contamination levels of astromaterials and hence the types of questions that can be answered about our solar system and the degree of precision that can be expected of those answers. Advanced curation was developed as a cross-disciplinary field to improve curation and acquisition practices in existing astromaterials collections and for future sample return activities, including meteorite and cosmic dust samples that are collected on Earth. These goals are accomplished through research and development of new innovative technologies and techniques for sample collection, handling, characterization, analysis, and curation of astromaterials. In this contribution, we discuss five broad topics in advanced curation that are critical to improving sample acquisition and curation practices, including (1) best practices for monitoring and testing of curation infrastructure for inorganic, organic, and biological contamination; (2) requirements for storage, processing, and sample handling capabilities for future sample
The temptation to equate environmental change with archaeologically observed events is always with us, and matching a climatic downturn with civilisation collapse is perhaps more attractive then ever. The archaeologically observed collapse of the Tiwanaku civilisation in the twelfth century AD has been specifically related to a prolonged drought which would have affected the people’s ability to produce food. However, a careful scrutiny of the data from ice cores and lake sediments persuades the author that no such drought can be inferred: the evidence for climatic change is of quite a different scale and order to the archaeological changes and cannot be used as an explanation of social events.
Genesis, a member of NASAs Discovery Mission program, is the world's first sample return mission since the Apollo program to bring home solar matter in ultra-pure materials. Outside the protection of Earth's magnetosphere at the Earth-Sun Lagrange 1 point, the deployed sample collectors were directly exposed to solar wind irradiation. The natural process of solar wind ion implantation into a highly pure silicon (Si) bulk composition array collector has been measured by spectroscopic ellipsometry and scanning transmission electron microscopy (STEM). Ellipsometry results show that bulk solar wind ions composed of approximately 95% H + , 4% He + and <1% other elements physically altered the first 59-63 nm of crystalline silicon substrate during 852.8 days of solar exposure. STEM analysis confirms that the solar accelerated ions caused significant strain and visible structural defects to the silicon structure forming a 60-75 nm thick irradiation damage region directly below the surface SiO 2 native oxide layer. Monte Carlo simulations of solar wind H, He, C, O, Ne, Mg, Si and Fe ion collisions in the Si collector with fluences calculated from the Genesis and ACE spacecrafts were used to estimate the energy deposited and Si vacancies produced by nuclear stopping in a flight-like Si bulk array collector. The coupled deposited energy model with the flown Genesis Si in situ measurements provides new insight into the basic principles of solar wind diffusion and space weathering of materials outside Earth's magnetosphere.
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