Die durch die Festkörperreaktion Adargestellte Titelverbindung kristallisiert in der Raumgruppe P43 mit Z ‐= 4. Ihre Struktur ist aus einem polymeren Kation, Z.[Hg‐,(HgBr)2As′4 ], und isoliert eingebauten Anionen, Bizßr" ,o, aufgebaut.
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