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Friction and wear behaviour of different concentrations of hex-boron nitride (h-BN) nanoparticles in engine oil of grade SAE 20W50 were studied at various loads. These tribological studies were conducted using a four-ball wear test machine and a pin-on-disc universal tribometer. Anti-wear properties of SAE 20W50 + h-BN were studied on the four-ball wear test machine as per ASTM D4172 standard. Friction and wear properties of SAE 20W50 + h-BN on piston ring and cylinder liner tribo-pair were studied using the universal tribometer. Nanoparticles of h-BN mixed in lubricant showed excellent tribological performance. In most of the cases, h-BN nanoparticles as additive reduced the wear loss by 30-70% at various loads. The minimum value of coefficient of friction (0.0401) was found with SAE 20W50 + 3 wt% of h-BN at normal load of 100 N. Scanning electron microscopy and Raman spectroscopy were used for characterisation of h-BN and wear scars.

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The performance of a lubricant greatly depends on the additives it involves. However, recently used additives produce severe pollution when they are burned and exhausted. Therefore, it is necessary to develop a new generation of green additives. Graphene oxide (GO) is considered to be environmentally friendly. The scope of this study is to explore the fundamental tribological behavior of graphene, the first existing 2D material, and evaluate its performance as a lubricant additive. The friction and wear behavior of 0.5 wt% concentrations of GO particles in ethanol and SAE20W50 engine oil on a hypereutectic Al-25Si alloy disc against steel ball was studied at 5 N load. GO as an additive reduced the wear coefficient by 60-80% with 30 Hz frequency for 120 m sliding distance. The minimum value of the coefficient of friction (0.057) was found with SAE20W50 C 0.5 wt% GO. A possible explanation for these results is that the graphene layers act as a 2D nanomaterial and form a conformal protective film on the sliding contact interfaces and easily shear off due to weak Van der Waal's forces and drastically reduce the wear. Scanning electron microscopy (SEM), energy-dispersive spectroscopy (EDS), and Raman spectroscopy were used for characterization of GO and wear scars.

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