This work reports a simple, novel, cost effective and eco-friendly electrolytic synthesis of silver nanoparticles using AgNO 3 as metal precursor. The synthesis rate is much faster than other methods and this approach is suitable for large scale production. They are characterized by XRD, SEM and FT-IR techniques to analyze size, morphology and functional groups. XRD studies reveal a high degree of crystallinity and monophasic Ag nanoparticles.Their particle size is found to be 24 nm and specific surface area (SSA) is 24 m 2 g -1 . Analysis of Ag nanoparticles SSA reports that increasing their SSA improves their antibacterial actions. Microbiology assay founds that Ag nanoparticles are effective against E.coli and B.megaterium bacteria.SSA of bacteria analysis reveals that it plays a major role while reacting with antimicrobial agents.

The preparation of biodegradable nanomaterials by blending starch nanocrystals with various polymer matrices are the most active research. This work reports aspect related to nano-sized particles of jackfruit seed. This approach is simple, faster, eco-friendly, cost effective and suitable for large scale production. X-Ray Diffraction studies analyze particles size, morphology, type of starch and degree of crystallinity. The particle size is found to be 12nm, specific surface area is 625 m 2 g -1 , contains A-type starch and 32% degree of crystallinity. A morphology index (MI) is developed from FWHM of XRD data to understand interrelationship of particle size and specific surface area. MI range is from 0.50 to 0.74. It is correlated with the particle size and specific surface area. It is observed that MI has direct relationship with particle size and an inverse relationship with specific surface area. __________________________________________________________________________________________

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This work reports, some of the features related to the room temperature superparamagnetic behaviours of lead nanoparticles. Such behaviours have not been discussed elaborately, in any literatures, so far. It is obvious from our studies that the superparamagnetic behaviours of Pb nanoparticles are surprising behaviours, since bulk Pb has diamagnetic behaviours. Hysteresis curve from Vibrating Sample Magnetometer study of Pb nanopowder (metal) serves some new observations. The successful calculations of values like magnetic size, saturation magnetization, coercive field, and remanent magnetism confirm its superparamagnetic nature and explore its potential application in various industries. This work throws some light on and helps further research.

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Copper (II) Hydroxide nano particles were synthesized via chemical co-precipitation method from Copper Sulphate and Sodium Hydroxide. Structural and compositional properties were characterized by XRD, SEM, FTIR and UV spectroscopy. XRD confirmed the preferential growth of Copper (II)Hydroxide nano particles that width is 33.42nm. The SEM image shows the synthesized Copper (II) Hydroxide show well crystallized particles with plate-like morphology. The FTIR spectrum is used to study the stretching and bending frequencies of molecular functional groups in the sample. From UV spectrum, the band gap of Copper (II) hydroxide nano particles is found to be 4.5 eV. From AAS studies, it is found that the absorbance is directly proportional to the concentration. The linear fit indicates that Copper (II) Hydroxide nanoparticles have been distributed in proper proportion.

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