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Partially stabilized zirconia (5Y-PSZ) has been widely used to manufacture indirect monolithic restorations, and the effect of finishing procedures on the optical and mechanical properties of these materials are still unclear. The purpose of this study was to evaluate the effect of staining, polishing and glazing on surface roughness, crystalline phase content, microhardness, fracture toughness, dynamic elastic modulus, three-point flexural strength, strain distribution, color (∆E00/∆L/∆a/∆b), and translucency before and after artificial accelerated aging (water spray and ultraviolet) of 5Y-PSZ. Bar-shaped and rectangle-shaped specimens of the 5Y-PSZ were prepared and divided into six groups, according to finishing procedure: GC (control), GS (staining), GG (glazing), GSG (staining and glazing), GP (polishing), GSP (staining and polishing). There was a significant difference between groups for surface roughness (p < 0.05), dynamic elastic modulus (p = 0.007), microhardness (p =  < 0.05), ∆E00 (p = 0.010), and ∆a (p = 0.008). GC presented higher cubic phase content, and the stained groups (GS, GSG and GSP) presented higher monoclinic content. The different finishing procedures affected roughness, dynamic elastic modulus, microhardness, and color of 5Y-PSZ; polishing being the finish that provides minors changes to the 5Y- PSZ. Accelerated artificial aging caused color change, regardless of finishing procedure used.

The purpose of this in vitro study was to compare the effect of staining, glazing, and polishing on the wear behavior of stabilized zirconia with 5 mol% of yttrium oxide (5Y-TZP) opposing 5Y-TZP, leucite-reinforced ceramic (LC), lithium disilicate (LD), and microhybrid composite resin (MCR). Hemispheres of 5Y-TZP were divided into six groups (n = 10) according to the finishing procedure: C (control), S (staining), G (glazing), P (polishings), SG (staining plus glazing), and SP (staining plus polishing). The two-body wear test (2BW) was performed (20 N load, at 2 Hz, until 300,000 cycles). Vertical height loss of hemispheres (VHL) and wear depth of restorative materials (WD) were analyzed using a profile projector and laser confocal microscope, respectively. Data of VHL and WD were analyzed using a generalized linear model by the Wald test and t post hoc test with the Bonferroni adjustment (α = 0.05). The staining, glazing, polishing, and restorative material had a significant effect (p < 0.05) on VHL and WD. Polishing reduced VHL opposing MCR, LC, and LD. There was an increase in WD to G opposing LD and SG opposing MCR. The 5Y-TZP presented the highest wear resistance, while MCR presented the lowest. Polishing was recommended to promote staining durability and decrease wear rates opposing MCR and LD.

Aim: The aim of this study was to evaluate fracture toughness by indentation method of three dental ceramics processed by heat pressing. The ceramics evaluated were fluorapatite glass ceramic (ZIR), glass ceramic containing leucite (POM) and leucite-reinforced glass ceramic (EMP). Materials and methods: Ninety disks (13mm of diameter x 4mm of thickness) and nine rectangular specimens (25x4x2mm) were made to evaluate, respectively, microhardness/fracture toughness (n=30) and elastic modulus (n=3). Samples were obtained by pressing ceramic into refractory molds. After polishing, Vickers microhardness was evaluated under 4,904N load for 20s. Elastic modulus was measured by impulse excitation technique. Data from microhardness and elastic modulus were used to calculate fracture toughness, after measuring crack length under 19,6N load applied for 20s. Results were evaluated by ANOVA and Tukey´s test. Results: Microhardness (VHN) of POM (637.9±53.6) was statistically greater (p<0.05) than ZIR (593.0±14. The results suggest that fluorapatite glass ceramic (ZIR) and leucite-reinforced glass ceramic (EMP) processed by heat pressing presented greater fracture toughness, improving clinical prognosis of metal free restorations.

Neves, pela amizade e incentivo. Cursar disciplinas ao lado de pessoas tão comprometidas e de potencial, me impulsionou a buscar ser melhor em cada seminário ministrado. Aos colegas de laboratório, Cristian Sbardelloto, Suleima Alves, Danilo Flamini, Renata Morais, Maria Paula Della Vechia e Bruna Tonin, pela convivência que tornou os dias de trabalho mais agradáveis. À amiga Renata Cardoso, pela amizade verdadeira, carinho e convivência desde a graduação.

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