This study investigated the influence of the surface treatment of curaua fibres (Ananas erectifolius) on the morphological, thermal and mechanical properties of polyester composites when the treated fibres (10 wt-%) were added. The following treatment agents were assessed: 10% Ba(OH) 2 , 14% Ca(OH) 2 , 5% NaOH, 10% KOH and 5% silane. The treatments removed amorphous components, thereby increasing the crystallinity of the fibres. Among the alkali treatments, KOH gave the highest crystallinity index (67.09%), Ca (OH) 2 had the best tensile strength (19 MPa) and Ca(OH) 2 treatment resulted in the highest composite thermal stability (315°C). Fibres treated with Ba(OH) 2 resulted in the composite with the greatest resistance to impact (55 vs 10 J m −1 for the neat matrix). Finally, the silane-treated fibres resulted in composites with a better performance than the other treatments. There was a prominent pattern of improved performance for the silane-treated fibre composites in all the analyses performed in this study.
Quality control to obtain composite laminates is frequently applied to synthetic fibers/epoxy prepregs. The gel time test, resin, volatiles and fiber content, drape measurement and tack tests together with water absorption capacity are methods currently employed. However, for natural fibers prepregs there is a gap in the literature, which makes their application difficult. Thus this work will investigate sisal fibers, which have low cost, high biodegradability and low specific weight, following the common methods to manufacture composites from natural fibers/epoxy prepregs. First, the prepregs were prepared by hand lay-up, aligning the fibers with epoxy, keeping 15% by weight content of fiber. After the quality control characterization, 3 mm thickness composite was prepared by using a press, and tensile tests and scanning electron microscopy (SEM) were applied. As a result, the resin fraction values and the solid content of the matrix showed little variation between the different samples. The natural fibers prepregs absorbed water quickly in the initial stage until reaching the saturation level. The NaOH-treated sisal/epoxy prepreg had a tension of 71.06 ± 8.28 kPa for the tack test and tensile strength of 69.24 ± 11.69 MPa. Finally, the NaOH-treated sisal 15 wt%/epoxy resulted in composites with a better performance than the neat epoxy resin. There was good adhesion between the fibers and matrix, as confirmed by SEM and mechanical tests.
A gestão de resíduos agrícolas e industriais é necessária para mitigar a poluição ambiental resultante de manejo de animais. Uma alternativa é utilizar resíduos para geração de energia, tornando um substrato com alto potencial poluidor ao meio ambiente em produto com maior valor agregado, como o biogás. O uso da Avaliação do Ciclo de Vida (ACV) para quantificar os impactos ambientais desses processos é uma ferramenta ideal e já consolidada mundialmente. Dentro das fases da ACV, a coleta de dados de inventário, definição das fronteiras e unidade funcional são pontos que devem ser explorados de maneira detalhada antes da construção do modelo. Quanto mais detalhado é o inventário, maior será a precisão de tomadas de decisão acerca dos processos analisados. Portanto, este estudo tem como objetivo elaborar um Inventário do Ciclo de Vida (ICV) da produção de biogás para geração de energia elétrica, utilizando o esterco do gado leiteiro como matéria-prima. A elaboração do ICV se deu por meio da coleta de dados locais em uma fazenda com atividades voltadas para a bovinocultura leiteira e com produção própria de biogás. Os resultados do ICV mostraram dados locais da produção diária de
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