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In the present work protonic forms of layeredn=1,3Ruddlesden-Popper oxides HLnTiO4and H2Ln2Ti3O10(Ln = La, Nd) were used as the starting point for soft chemistry synthesis of two series of perovskite-like compounds by acid leaching and exfoliation, promoted by vanadyl sulfate. The last route leads to the nanostructured VO2+containing samples. Characterization by SEM, powder XRD, and TGA has been performed for the determination of the structure and composition of synthesized oxides.