Chemical protective clothing (CPC) has become mandatory when performing various tasks to ensure user protection and prevent chemicals from contacting the skin and causing severe injuries. In addition to protection, there is a need to develop a simple mechanism that can be attached to CPC and be capable of detecting and alerting the user to the presence of harmful chemical agents. In this study, a double-sensor strategy was investigated, using six different pH indicators stamped on cotton and polyester knits to detect acidic and alkaline substances, both liquid and gaseous. Functionalized knits underwent microscopic characterization, air permeability and contact angle evaluation. All samples exhibited hydrophobic behavior (contact angle > 90°) and air permeability values above 2400 L/min/cm2/bar, with the best condition demonstrating a contact angle of 123° and an air permeability of 2412.5 L/min/cm2/bar when the sensor methyl orange and bromocresol purple (MO:BP) was stamped on polyester. The performed tests proved the functionality of the sensors and showed a visible response of all knits when contacting with different chemicals (acids and bases). Polyester functionalized with MO:BP showed the greatest potential, due to its preeminent color change. Herein, the fiber coating process was optimized, enabling the industrial application of the sensors via a stamping method, an alternative to other time- and resource-consuming techniques.
Biological hazards can be defined as substances that endanger the life of any living organism, most notably humans, and are often referred to as biohazards. Along with the use of personal protective equipment (PPE), early detection of contact is essential for the correct management and resolution of a biological threat, as well as lower mortality rates of those exposed. Herein, Prussian blue (PB) was evaluated as a functional compound applied on polyester knits to act as an on-site sensor for bacteria detection. In order to study the best compound concentration for the intended application, polymeric solutions of 0.5, 1 and 2 g/L were developed. The three conditions tested displayed high abrasion resistance (>2000 cycles). The bacterial sensing capacity of the coated knits was assessed in liquid and solid medium, with the functionalised substrates exhibiting the capability of detecting both Gram-positive and Gram-negative bacteria and changing colours from blue to white. Evaluation of water repellence and chemical penetration resistance and repellence was also performed in polyester functionalised with PB 0.5 and 1 g/L. Both knits showed a hydrophobic behaviour and a capacity to resist to penetration of chemicals and level 3 repellence effect for both acid and base chemicals.
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Control of food spoilage is a critical concern in the current world scenario, not only to ensure the quality and safety of food but also to avoid the generation of food waste. This paper evaluates a dual-sensor strategy using six different pH indicators stamped on cardboard for the detection of spoilage in three different foods: beef, salmon, and strawberries. After function validation and formulation optimizations in the laboratory, the halochromic sensors methyl orange and bromocresol purple 2% (w/v) were stamped on cardboard and, in contact with the previously mentioned foods, were able to produce an easily perceptible signal for spoilage by changing color. Additionally, when it comes to mechanical characterization the inks showed high abrasion (>100 cycles) and adhesion resistance (>91%).
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