Acetone is a main respiratory marker for diabetic patients. In this paper, P-type NiO nanofibers were prepared by electrospinning and used for the detection of acetone gas. NiO nanofibers were characterized by SEM and XRD. The uniform NiO nanofibers with face-centered cubic structure was obtained. The working temperature of NiO nanofibers was optimized, and the optimal operating temperature is 220°C. The response-recovery curve was tested, and the response and recovery time is 24.6 s and 610 s respectively. The response to different concentrations of acetone was also analyzed, and the detection limit was 100 ppb. These results show that NiO nanofibers based on electrospinning have potential applications in the respiratory testing of diabetes.
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