Nylon 6/Chitosan membranes were fabricated by electrospinning onto a Millipore glass fiber filter to produce nanofibrous filter. Scanning electron microscopy (SEM) and water contact angle (WCA) were done to characterize the produced filter. Filter removal capability (adsorption) for metal ions was investigated for lead nitrate (Pb(NO3)2) and sodium chloride (NaCl). The antibacterial effect of the Nylon 6/Chitosan was investigated for Escherichia coli. Removal optimum values for Pb(NO3)2 and NaCl reached 87% and 75%, respectively. This research demonstrated that Nylon 6/Chitosan nanofibrous membrane has an enormous applicable potential removal for metal ions from aqueous solutions, antibacterial activity reaching 96%, and reasonable inhibition zone against Escherichia coli (E. coli).
Bacterial water pollution is a genuine general wellbeing concern since it causes various maladies. Antimicrobial nanofibers can be integrated by incorporating nanobiocides, for example, silver nanoparticles into nanofibers. Nylon 6 was dissolved in formic acid at a concentration of (25 wt. %) and tough antibacterial (AgNO3/Nylon) nanofibers were produced utilizing electrospinning system. Polymer solution was tested before accomplishing electrospinning process to acquire its surface tension, electric conductivity and viscosity, where every one of those parameters increased relatively with increasing concentration of (AgNO3) additions. SEM and EDX spectra were utilized to focus on the morphology, surface elemental membrane, fibers and porosize diameters. The resulted nanofiber membrane has an average fiber diameter of 139 nm for pure nylon 6 and 247 nm for (1.2 wt. % AgNO3/Nylon). The resultant polymer membrane was then tested for their ability to destroy microorganisms in water; antimicrobial tests showed that the prepared nanofibers have a high bactericidal effect against Escherichia Coli Bacteria with inhibition zone (10 mm) and antibacterial activity (99%). Likewise, these results highlight the potential utilization of these nanofibrous mats as antimicrobial agents.
This paper studies the electroless (Ni-P) deposition which is used in different engineering applications due to their ability to modify and enhance the surface properties of the steel substrate. The electroless plating process was used to prepare (Ni-Cu-P), (Ni-P) and (Ni-Cu-P/Nano TiO2) alloys in this research. Deposition process parameters based on (L28) Taguchi orthogonal configuration with three process parameters, viz., stirring speed, temperature, time, are designed for optimum microhardness. Under the Taguchi series, the microhardness activity of electroless (Ni-P-TiO2) nanocomposite deposition was measured. The findings revealed that the integration of TiO2 into the coating allows micro-hardness cause an increase. Finally, optimum conditions were achieved as A2B1C2 (i.e. Speed of stirring = 1000 r.p.m, Temperature = 90 °C and Time = 70 min).
In this research, (MOORA) approach based– Taguchi design was used to convert the multi-performance problem into a single-performance problem for nine experiments which built (Taguchi (L9) orthogonal array) for carburization operation. The main variables that had a great effect on carburizing operation are carburization temperature (oC), carburization time (hrs.) and tempering temperature (oC). This study was also focused on calculating the amount of carbon penetration, the value of hardness and optimal values obtained during the optimization by Taguchi approach and MOORA method for multiple parameters. In this study, the carburization process was done in temperature between (850 to 950 ᵒC) for 2 to 6 hours. Quenching was done for the specimens after heat treatments in furnace chamber by using different quench solutions, water, salt and polyvinyl alcohol. Analysis of variances - (ANOVA) were performed for nine experiments in order to optimize the problem that was associated with multiple criteria (parameter) to achieve maximum hardness and depth penetration. The program results showed that the optimum conditions are carburization temperature (950 oC), carburization time (2 hrs.), tempering temperature (200oC), tempering time (10 hrs.), and activator (10 wt. %). Furthermore, the best quenching media was the polyvinyl alcohol.
In this research, a multi-response optimization based on Taguchi method is proposed for friction stir welding (FSW) process for (2024-T3) aluminum alloy. Three different shoulder diameters of tools with tapered pin geometry of (12, 14 and 14 mm) with variable rotation speed (710, 1000 and 1400 rpm) and welding speed of (40, 56 and 80 mm/min), three different tilting angles of (1, 2 and 3 degree) and three welding direction of (1, 2 and 3 passes). The results of this work showed the single optimization by using (Taguchi method) at the optimum condition for the tensile strength and yield strength were (365 MPa) and (258 MPa) respectively; at the parameters: shoulder diameter (14 mm), rotation speed (1400 rpm), linear speed (40 mm/min), tilting angle ((3°) for tensile strength and (1°) for yield strength) and welding direction (3 passes). The results of multi-response optimization for (FSW) process at the optimum condition for tensile strength and yield strength were (371 MPa) and (268 MPa), respectively; at the parameters: shoulder diameter (14 mm), rotation speed (1400 rpm), linear speed (40 mm/min), tilting angle (3°) and welding direction (3 passes).
The purpose of this study is designate quenching and tempering heat treatment by using Taguchi technique to determine optimal factors of heat treatment (austenitizing temperature, percentage of nanoparticles, type of base media, nanoparticles type and soaking time) for increasing hardness, wear rate and impact energy properties of 420 martensitic stainless steel. An (L18) orthogonal array was chosen for the design of experiment. The optimum process parameters were determined by using signal-to-noise ratio (larger is better) criterion for hardness and impact energy while (Smaller is better) criterion was for the wear rate. The importance levels of process parameters that effect on hardness, wear rate and impact energy properties were obtained by using analysis of variance which applied with the help of (Minitab18) software. The variables of quenching heat treatment were austenitizing temperature (985 C˚,1060 C˚),a soaking times (50,70 and 90 minutes) respectively, Percentage of volumetric fractions of nanoparticles with three different levels(0.01, 0.03 and 0.08 %) were prepared by dispersing nanoparticles that are (α-Al2O3,TiO2 and CuO) with base fluids (De-ionized water, salt solution and engine oil).The specimens were tempered at 700°C after quenching of nanofluids for (2 hours).The results for ( S/N) ratios showed the order of the factors in terms of the proportion of their effect on hardness, and wear rate properties as follow: Austenitizing temperature ( 1060 C˚),Type of base media (salt solution), Nanoparticles type (CuO), Percentage of nanoparticles (0.08%) and Soaking time(90min) was the least influence while for the impact energy were as follows: Type of base media (oil), Austenitizing temperature (985C˚), Percentage of nanoparticles (0.01%), Nanoparticles type (α-Al2O3) and last soaking time (50min).
The current work is conducting an experimental investigation into the effect of those technical parameters, called nanomaterial, bath temperature and plating time on the micro-hardness and corrosion rate of electroless plated low carbon steel undergoing electroless deposition operation. It was used to prepare (Ni-P/ Nano TiO2), (Ni-P/ Nano Al2O3) and (Ni -P/ Nano SiO2) alloys in this research. The Taguchi design is used to describe the variations located within the corrosion and mechanical properties. To achieve a comprehensive study, a Taguchi-based design was used to account for all applicable combinations of factors. Experimental models had been advanced that linking the response and method parameters to the results of those experiments. Validation of these models is done using analysis of variance (ANOVA). The desirability function is used to simultaneously optimize all the response. Finally, the optimum combination of method parameters resulting (bath temperature=90 oC, plating time =120 min. and Nanomaterial=(Al2O3)), nanomaterial was observed to be the major process parameter on the responses of the electroless-plated low carbon steel with an impact ratio of (47%) based on the (ANOVA) results.
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