X-RayCrystal Structures of y,-Chloro-(tris[trichloro(thiosemicarbazide)bismuth ( II I)] ) [ t r is( t h iosemica r bazide) bismuth ( II I)] Hexachloro bismuthate(1ii) Chloride and catena-y-Chloro-dichlorobis(ethy1enethiourea)bismuth( 111)
The compound 3-(2-pyridyl)triazolo[l,5-a] pyridine (L) was synthesized under mild conditions by refluxing equimolar amounts of hydrazine and di-2-pyridyl ketone in methanol-water. It has been characterized by X-ray diffraction and used as a ligand in two metal complexes, [ML,(OH,),][NO,], ( M = Cu or Co). The crystal structure of the copper derivative, which is the first example of a triazolopyridine complex, has also been determined.
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