calculated from the oxidation potential versus the internal standard of ferrocene/ferrocenium and the I p (5.43 eV) so obtained for PATPD was in good agreement with the I p reported for TPD based materials (5.4 eV determined by UV-PES) [26].Absorption Spectra: Absorption spectra of the samples were measured with a Cary 5G spectrophotometer.Dark Conductivity and Photoconductivity: Steady-state conductivity properties were determined in the dark. To measure the steadystate dark conductivity, an electric field (E a ) was applied and the current (i dark ) was measured. To assure steady-state conditions a dwell time of 15 s between each reading was used. The applied electric field was swept from 0 to 76 V lm ±1 over a period of 7 min. The current was measured using a Keithley 6517A electrometer.Four-Wave Mixing and Exposure Dependent Transient Four-Wave Mixing Experiments: A detailed discussion about the experimental set-up is given in [22].
In the spray cooling of a heated surface, variations in the surface texture influence the flow field, altering the maximum liquid film thickness, the bubble diameter, vapor entrapment, bubble departure characteristics, and the ability to transfer heat. A new method for determining and designating the surface texture is proposed, and the effects of surface roughness on evaporation/nucleation in the spray cooling flow field studied. A one-dimensional Fourier analysis is applied to determine experimentally the surface profile of a surface polished with emery paper covering a spectrum of grit sizes between 0.3 to 22 μm. Heat transfer measurements for liquid flow rates between 1 to 5 l/h and air flow rates between 0.1 to 0.4 l/s are presented. Maximum heat fluxes of 1200 W/cm2 for the 0.3 μm surface at very low superheats were obtained.
An experimental study to determine the effect of liquid and secondary gas flow in droplet impingement cooling is presented. The nucleate boiling regime in particular is analyzed. A correlation to predict the Nusselt number based on the liquid film thickness is derived and compared with the experimental data.
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