The effects of the titanium and oxygen concentration on the characteristics of inclusions and microstructure in low carbon wrought steels were investigated. Increasing the titanium concentration from 48 to 120 ppm promoted the formation of TiN particles and decreased the prior austenite grain size. The fraction of intragranular ferrite in the microstructure was relatively unchanged. When the oxygen concentration was increased from 50 to 130 ppm, the volume fraction and the number of inclusion increased. However, the fraction of intragranular ferrite in microstructures decreased abruptly above 80 ppm because the allotriomorph ferrite phase at the prior austenite grain boundary began to form.
Technical investigation to figure out the problems arising during in-situ heating electron backscatter diffraction (EBSD) analysis inside scanning electron microscopy (SEM) was carried out. EBSD patterns were successfully acquired up to 830 o C without degradation of EBSD pattern quality in steels. Several technical problems such as image drift and surface microstructure pinning were taking place during in-situ experiments. Image drift problem was successfully prevented in constant current supplying mode. It was revealed that the surface pinning problem was resulted from the TiO 2 oxide particle formation during heating inside SEM chamber. Surface pinning phenomenon was fairly reduced by additional platinum and carbon multi-layer coating before in-situ heating experiment, furthermore was perfectly prevented by improvement of vacuum level of SEM chamber via leakage control. Plane view in-situ observation provides better understanding on the overall feature of recrystallization phenomena and cross sectional in-situ observation provides clearer understanding on the recrystallization mechanism.
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