In the present work, the microstructure, texture, mechanical properties as well as hot deformation behavior of a Mg-2Zn-1Al-0.3Ca sheet manufactured by twin roll casting were investigated. The twin roll cast state reveals a dendritic microstructure with intermetallic compounds predominantly located in the interdendritic areas. The twin roll cast samples were annealed at 420 °C for 2 h followed by plane strain compression tests in order to study the hardening and softening behavior. Annealing treatment leads to the formation of a grain structure, consisting of equiaxed grains with an average diameter of approximately 19 µm. The twin roll cast state reveals a typical basal texture and the annealed state shows a weakened texture, by spreading basal poles along the transverse direction. The twin roll cast Mg-2Zn-1Al-0.3Ca alloy offers a good ultimate tensile strength of 240 MPa. The course of the flow curves indicate that dynamic recrystallization occurs during hot deformation. For the validity range from 250 °C to 450 °C as well as equivalent logarithmic strain rates from 0.01 s−1 to 10 s−1 calculated model coefficients are shown. The average activation energy for plastic flow of the twin roll cast and annealed Mg-2Zn-1Al-0.3Ca alloy amounts to 180.5 kJ/mol. The processing map reveals one domain with flow instability at temperatures above 370 °C and strain rates ranging from 3 s−1 to 10 s−1. Under these forming conditions, intergranular cracks arose and grew along the grain boundaries.

In the present work, the microstructure and texture of a Mg–6.8Y–2.5Zn–0.4Zr sheet manufactured by twin-roll casting were investigated. The twin-roll cast state consisted of two apparent phases: the α-Mg matrix, which was made up of dobulites with an average grain size of approximately 50 µm and the LPSO (long-period stacking ordered) phase, which formed network-like precipitates along the grain boundaries. After twin-roll casting, annealing was carried out under conditions of different temperatures ranging from 450 °C to 525 °C and holding times between 2 h and 24 h. It was found that heat treatment led to the formation of a microstructure in which grains were apparent. Furthermore, it could be observed that high temperatures > 500 °C led to changes in the morphology of the LPSO structures. On one hand, the network-like structure dissolved while, on the other hand, both rodlike and blocky LPSO phases precipitated predominantly at the grain boundaries of the α-Mg matrix. This process was fostered by high temperatures and long holding times.

No abstract

Das Teilprojekt B3 des SFB 692 hat sich zum Ziel gesetzt, Aluminium/Magnesium‐Verbunde hinsichtlich seiner mechanischen Festigkeitseigenschaften und bruchmechanischen Kenngrößen zu analysieren. Des Weiteren soll die entstandene Grenzschicht in einem numerischen Modell abgebildet werden. Im folgenden Artikel werden die wesentlichen Erkenntnisse des Teilprojektes dargelegt. Es wurden verschiedene Faktoren untersucht, welche die Eigenschaften der Grenzschicht beeinflussen. Es zeigt sich, dass die Verbundqualität und die Festigkeit der Grenzschicht von einer Reihe von Größen abhängen, die maßgeblich im Prozess der Halbzeugherstellung, dem hydrostatischen und indirekten Strangpressen, begründet sind. Wird eine qualitativ einwandfreie Grenzschicht zwischen beiden Verbundpartnern erzeugt, weist dieses Interface eine hohe Festigkeit auf. Darüber hinaus wird gezeigt, wie sich die Verbunde in verschiedenen Temperaturbereichen unter Belastung verhalten. Des Weiteren wird das Versagensverhalten des Verbundes numerisch abgebildet.

The changes of ecological awareness of political initiatives give new rules for economy and industry with the aim to support environmental friendly technology. Research projects are focusing on lightweight designs especially in automotive and aerospace industry. This paper deals with the results of the application of lightweight materials, in detail with aluminum-magnesium-compounds and its manufacturing process. Thereby, the process chain from the production of semi-finished parts and the first subsequent process will be explained in detail with focusing on the modification of the intermetallic interface. The combination of hydrostatic co-extrusion and subsequent performed forging is an auspicious approach for the production of lightweight parts made of Al-Mg-compounds. In this contribution the main influencing parameters, experimental and numerical work, interface properties as well as the process analysis will be explained in detail.

Deformation behavior of an as-cast Mg-6.8Y-2.5Zn-0.4Zr alloy during plane strain compression was characterized in present work by high-temperature testing. Based on the experimental data, the values of strain rate sensitivity, efficiency of power dissipation and the instability parameter under the condition of various hot working parameters were investigated. Processing maps were established by superimposing the instability map over the power dissipation map, this being connected with microstructural evolution analysis in the hot deformation processes. Accompanied microstructure characterization of the binary α-Mg/ Long Period Stacking Ordered (LPSO) microstructure reveals that the flow behavior is related to the deformation mechanisms. At lower temperatures (350 – 400 °C) formation of kink bands is observed, which normally occur when deformation twinning is inhibited and other slip systems are strongly hindered by the complex LPSO structures. Dynamic recrystallization (DRX) was initiated at higher temperatures above 400 °C, influencing the softening behavior of the material significantly. DRX was the main softening mechanism when deformation takes place at 500 °C and the kink band deformation decreased.

This paper provides an analysis of a co-extrusion process. The compound consists of the sleeve material, aluminum, and the core material, magnesium. It is imperative to produce impeccable compounds without cracks in the interface. Therefore, a simple indicating value for damaging effects during the process is necessary. In the numerical simulation the compound quality is noticeable by the current macro mechanical criterion of axial strain difference. A statistical analysis verifies this criterion as an adequate quality criterion. By means of this criterion it is possible to define a stable process window for the co-extrusion process.

In this work, the deformation behaviour of a twin-roll cast (TRC) Mg-6.8Y-2.5Zn-0.4Zr alloy during plane strain compression was characterised by high-temperature testing. Based on the experimental data, the values of strain-rate sensitivity, the efficiency of power dissipation and the instability parameter were investigated under the conditions of various hot deformation parameters. In contrast to conventionally cast material, no lamellae of the LPSO (long period stacking ordered) phase were precipitated in the magnesium matrix after TRC. The precipitation of fine lamellar LPSO phases only occurred during cooling to forming temperature after the heat treatment. Dynamic recrystallization (DRX) hardly occurred during deformation at temperatures between 350 °C and 400 °C. This can be attributed to the precipitation of the lamellar LSPO phases, which contribute to retardation of the DRX process. At higher deformation temperatures and strain rates DRX is pronounced and the twin-induced (TRDX) as well as continuous dynamic recrystallization could be identified as the dominant softening mechanisms. The processing maps were established by superimposing the instability map over the power dissipation map, this being associated with microstructural evolution analysis in the hot deformation processes. Two instability zones could be recognised for the twin-roll cast and heat-treated Mg-6.8Y-2.5Zn-0.4Zr alloy: (1) 350 °C to 460 °C and 0.01 s−1 to 0.3 s−1 and (2) 485 °C to 525 °C and 2.5 s−1 to 10 s−1, where deformation is not favourable.